Vapor management take off rates question

Distillation methods and improvements.

Moderator: Site Moderator

copperlover1
Swill Maker
Posts: 250
Joined: Mon Jan 06, 2014 8:59 am

Vapor management take off rates question

Post by copperlover1 »

Hello all. I am looking to see what I need to change to increase my take off rate. Currently running 2" VM . 2' packed with ss scrubies. 1" take off to 1" gate valve reduced to 1/2 condenser. 15 gallon keg on propane burner. Run time. 15 gallon gerber wash fermented to very dry wine. 1 hour heat up to temp. Reduce heat to 1/4 open gas valve.15 minutes stabilize.take off fore shots. Close and 15 minutes stabilize. Open gate valve all the way. Collect about 7/8 qt per hour at 95%. Collect about 6-1/2 qts at 95% and temp never changes once. Temp goes up proof goes down end of run. So what can I change to get a better take off rate?
Attachments
image.jpg
User avatar
Bushman
Admin
Posts: 18006
Joined: Tue Mar 30, 2010 5:29 am
Location: Pacific Northwest

Re: Vapor management take off rates question

Post by Bushman »

Diameter equals speed, height purity. I ran a 2" VM for years and a typical 11-12 gallon charge would take between 12-17 hours depending on how I ran it. I went to a 4" CM and my runs are 3-5 hours with the same charge.
User avatar
DAD300
Master of Distillation
Posts: 2839
Joined: Wed Mar 02, 2011 11:46 am
Location: Southern U.S.

Re: Vapor management take off rates question

Post by DAD300 »

The closer your takeoff dia gets to the column dia will allow for higher takeoff.

You are currently operating at approx 4:1, reflux: takeoff, max.

A 2" column with a 2" takeoff will allow approx 1:1 reflux:takeoff.
CCVM http://homedistiller.org/forum/viewtopi ... d#p7104768" onclick="window.open(this.href);return false;" rel="nofollow
Ethyl Carbamate Docs viewtopic.php?f=6&t=55219&p=7309262&hil ... e#p7309262
DSP-AR-20005
User avatar
skow69
Site Donor
Site Donor
Posts: 3230
Joined: Tue Dec 06, 2011 3:03 am
Location: Cascadia

Re: Vapor management take off rates question

Post by skow69 »

when the vapor gets to the tee the stream splits in proportion to the size of the pipes. You are giving it a choice of a 1" to product takeoff or a 2" to the reflx condenser.
1" cross section = 0.79sq.in.
2" cross section = 3.14sq.in.
So 80% of your vapor is going up to the RC and back down the column. 20% is going out the takeoff.
So you can
1) increase the takeoff cross section,
2) restrict the path to the RC, or
3) create some turbulance and hope for the best.

Frankly, I think your 7 - 8 qts. per hour estimate is pretty optimistic.
Distilling at 110f and 75 torr.
I'm not an absinthe snob, I'm The Absinthe Nazi. "NO ABSINTHE FOR YOU!"
copperlover1
Swill Maker
Posts: 250
Joined: Mon Jan 06, 2014 8:59 am

Re: Vapor management take off rates question

Post by copperlover1 »

That's a fraction 7/8 ths of a quart per hour. Sorry. I am really just looking to hit maybe 1-1/2 qts per hr. I would like to start after I eat breakfast and finish before I eat dinner.
User avatar
skow69
Site Donor
Site Donor
Posts: 3230
Joined: Tue Dec 06, 2011 3:03 am
Location: Cascadia

Re: Vapor management take off rates question

Post by skow69 »

Oh, in that case it's just depressing.

Sorry, but your options are still the same. You're just not taking off much product. Bumping up to a 2" takeoff valve would probably better than double your output.
Distilling at 110f and 75 torr.
I'm not an absinthe snob, I'm The Absinthe Nazi. "NO ABSINTHE FOR YOU!"
User avatar
skow69
Site Donor
Site Donor
Posts: 3230
Joined: Tue Dec 06, 2011 3:03 am
Location: Cascadia

Re: Vapor management take off rates question

Post by skow69 »

Or you could probably get almost the same improvement and save a few bucks by replacing your 2x2x1 tee with a 1x1x1 and two 2x1 reducers. Know what I mean?
Distilling at 110f and 75 torr.
I'm not an absinthe snob, I'm The Absinthe Nazi. "NO ABSINTHE FOR YOU!"
User avatar
DAD300
Master of Distillation
Posts: 2839
Joined: Wed Mar 02, 2011 11:46 am
Location: Southern U.S.

Re: Vapor management take off rates question

Post by DAD300 »

skow69 wrote:Oh, in that case it's just depressing.
You made me laugh...sorry...

If you had the 2" takeoff, you would get close to 2 quarts an hour.

Dumping the valve and it's restriction would help a little, but would require you rework the top to CCVM.
CCVM http://homedistiller.org/forum/viewtopi ... d#p7104768" onclick="window.open(this.href);return false;" rel="nofollow
Ethyl Carbamate Docs viewtopic.php?f=6&t=55219&p=7309262&hil ... e#p7309262
DSP-AR-20005
User avatar
bearriver
Site Donor
Site Donor
Posts: 4442
Joined: Fri Nov 22, 2013 10:17 pm
Location: Western Washington

Re: Vapor management take off rates question

Post by bearriver »

skow69 wrote:Or you could probably get almost the same improvement and save a few bucks by replacing your 2x2x1 tee with a 1x1x1 and two 2x1 reducers. Know what I mean?
I would go with this design. Hookline has pictures of it in his pdf file "Some still drawings", for the visual learners.

7/8 of a quart per hour is very slow, but the reasons for that have been explained well. Address those design changes and see where that gets you. If it's still not enough then start fresh and build a larger diameter column.

Experimenting with different packing arrangements would be a good thing also. Rad gets impressive takeoff rates from a tiny column using marbles.
User avatar
still_stirrin
Master of Distillation
Posts: 10344
Joined: Tue Mar 18, 2014 7:01 am
Location: where the buffalo roam, and the deer & antelope play

Re: Vapor management take off rates question

Post by still_stirrin »

DAD300 wrote:The closer your takeoff dia gets to the column dia will allow for higher takeoff.

You are currently operating at approx 4:1, reflux: takeoff, max.

A 2" column with a 2" takeoff will allow approx 1:1 reflux:takeoff.
Hey, I'm thinking that area is pi x R squared. So the minimum reflux ratio from 2" to 1/2" is 1/(1/4)squared = 16:1 (I think, if my math is correct).

My 2" to 1" has a minimum RR of 1/(1/2)^2 = 4:1.

No wonder your take off is so slow.
ss
My LM/VM & Potstill: My build thread
My Cadco hotplate modification thread: Hotplate Build
My stock pot gin still: stock pot potstill
My 5-grain Bourbon recipe: Special K
copperlover1
Swill Maker
Posts: 250
Joined: Mon Jan 06, 2014 8:59 am

Re: Vapor management take off rates question

Post by copperlover1 »

Just want to say thanks. To everyone who replyed with all the great info. I am thinking CCVM. No valve to buy and I have lots of 2" copper to work with. Will I have to make my take off condenser bigger?
hellbilly007
Site Donor
Site Donor
Posts: 582
Joined: Fri Aug 03, 2012 10:59 am
Location: Never one place very long

Re: Vapor management take off rates question

Post by hellbilly007 »

Your 1" take off valve is being choked down by your 3/4" over 1/2" liebeg. If you increase the diameter of your condensor to 1" it will increase your take off. By the time you buy the fittings to build a larger condensor you could build a CCVM for less and have even faster take off.
copperlover1
Swill Maker
Posts: 250
Joined: Mon Jan 06, 2014 8:59 am

Re: Vapor management take off rates question

Post by copperlover1 »

Won't I need a bigger Liebig on my take off with a CCVM?
User avatar
still_stirrin
Master of Distillation
Posts: 10344
Joined: Tue Mar 18, 2014 7:01 am
Location: where the buffalo roam, and the deer & antelope play

Re: Vapor management take off rates question

Post by still_stirrin »

copperlover1 wrote:Won't I need a bigger Liebig on my take off with a CCVM?
Possibly, if you're trying to minimize the reflux ratio.

My VM runs 2" column to 1 1/2" takeoff then reduces to 1" through the control valve. From there it's 1" to the 7 x 3/8" shotgun. I can run it at 1 pint every 12 minutes with a 2kW input.

So you may need a faster (larger diameter) product condenser input, if you want to run faster. Size matters! (in this case).
ss
My LM/VM & Potstill: My build thread
My Cadco hotplate modification thread: Hotplate Build
My stock pot gin still: stock pot potstill
My 5-grain Bourbon recipe: Special K
hellbilly007
Site Donor
Site Donor
Posts: 582
Joined: Fri Aug 03, 2012 10:59 am
Location: Never one place very long

Re: Vapor management take off rates question

Post by hellbilly007 »

Yes, you'll need a larger diameter condensor. I forgot to mention that earlier. A 2" shotgun condensor would be ideal.

If you're not looking to get too involved, a larger diameter liebeg with copper scrubbie stuffed inside would a quick fix for running faster.
User avatar
T-Pee
Site Donor
Site Donor
Posts: 4355
Joined: Mon Feb 18, 2013 9:20 pm
Location: The wilds of rural California

Re: Vapor management take off rates question

Post by T-Pee »

Don't forget some kind of turbulator inside the external jacket and a bit of scrubbie inside the takeoff line.

tp
Last edited by T-Pee on Wed Oct 29, 2014 12:17 pm, edited 1 time in total.
User avatar
DAD300
Master of Distillation
Posts: 2839
Joined: Wed Mar 02, 2011 11:46 am
Location: Southern U.S.

Re: Vapor management take off rates question

Post by DAD300 »

No you don't need to increase the dia of your liebig. However if your takeoff increases to something your PC can't condense, you may need to increase the length.

Keep the inside dia of the takeoff 2" from "T" to 90 deg elbow...once you make the drop from 2" elbow the dia becomes of little importance. Keep the horizontal out of the "T" as short as possible.

As the vapor cools and collapses to liquid it actually helps evacuate it through the Product Condenser and the size is less relevant.

I have used the same condenser(s) on 2", 3" and 4". The condenser is not a restriction.

My 4" CCVM is 4" from column to 90 deg elbow down. 4"-2" reducer to Product condenser and 1/2" out of product condenser. Nothing past the downward bend will slow the vapor or liquid.
Attachments
3" column, 3" T and 3" elbow
3" column, 3" T and 3" elbow
3 inch.jpg (74.27 KiB) Viewed 4665 times
CCVM http://homedistiller.org/forum/viewtopi ... d#p7104768" onclick="window.open(this.href);return false;" rel="nofollow
Ethyl Carbamate Docs viewtopic.php?f=6&t=55219&p=7309262&hil ... e#p7309262
DSP-AR-20005
rad14701
retired
Posts: 20865
Joined: Wed Dec 19, 2007 4:46 pm
Location: New York, USA

Re: Vapor management take off rates question

Post by rad14701 »

VM branch sizing is only critical before the product condenser... If the product condenser is efficient enough for the amount of heat remaining in the take off branch then size is irrelevant... But if the path to the condenser is restricted for any reason, that is the contributing factor when it comes to the maximum output... So if you can get enough vapor to the 3/4" over 1/2" product liebig it will knock it down efficiently, just like they do when running stripping runs with a pot still ...
hellbilly007
Site Donor
Site Donor
Posts: 582
Joined: Fri Aug 03, 2012 10:59 am
Location: Never one place very long

Re: Vapor management take off rates question

Post by hellbilly007 »

My apologies Copperlover1, I stand corrected. Thanks DAD and Rad for chiming in. I didn't consider the vapor collapsing.
copperlover1
Swill Maker
Posts: 250
Joined: Mon Jan 06, 2014 8:59 am

Re: Vapor management take off rates question

Post by copperlover1 »

No problem. Going to mill out a 2" hole where my 1" hole is. Solder in 2" pipe. Than reduce down to my Liebig. Than remove the reflux condenser and replace with just an extension pipe that I will put in a wound up condenser that I can slide up and down. Big question. I have been looking and can see where to put the thermometer. Do I need 2. One on the take off and one in the column ? Will do a drawing first.
bellybuster
Master of Distillation
Posts: 4490
Joined: Tue Dec 18, 2012 5:00 pm

Re: Vapor management take off rates question

Post by bellybuster »

I'm incredibly impressed you get 95% from 2' of column. You speed things up I bet you'll lose those impressive numbers
copperlover1
Swill Maker
Posts: 250
Joined: Mon Jan 06, 2014 8:59 am

Re: Vapor management take off rates question

Post by copperlover1 »

I couldn't believe it either. But that what my alcohlometer read. The hearts were super clean too. It's awesome when you go to smell in the jar and you bump you lips to it. Alchol Feels like is walking across them it so lite an clean
copperlover1
Swill Maker
Posts: 250
Joined: Mon Jan 06, 2014 8:59 am

Re: Vapor management take off rates question

Post by copperlover1 »

Ok going to try this first. Mill the 2" hole in the side of my tee . 2" to 1" valve than Liebig . Thermometer in takeoff section. Marbles in column instead of ss scrubies.
Attachments
image.jpg
User avatar
Bushman
Admin
Posts: 18006
Joined: Tue Mar 30, 2010 5:29 am
Location: Pacific Northwest

Re: Vapor management take off rates question

Post by Bushman »

bellybuster wrote:I'm incredibly impressed you get 95% from 2' of column. You speed things up I bet you'll lose those impressive numbers
True about speeding things up. I have a 2" VM and getting 95% is pretty typical when running it properly, much easier than my 4" CM.
User avatar
DAD300
Master of Distillation
Posts: 2839
Joined: Wed Mar 02, 2011 11:46 am
Location: Southern U.S.

Re: Vapor management take off rates question

Post by DAD300 »

Your new drawing is an improvement, but not much.

1-to get the greatest benefit from the 2" takeoff, you need to make the downward turn in 2".
2-if the valve is lower, after the bend, it will pool some amount of liquid when closed.
3-switching to marbles will require longer equilizing/refluxing to maintain the high ABV, thus again slowing your takeoff. Basically you'll be closing the valve down to offset the reduce column resolution.
CCVM http://homedistiller.org/forum/viewtopi ... d#p7104768" onclick="window.open(this.href);return false;" rel="nofollow
Ethyl Carbamate Docs viewtopic.php?f=6&t=55219&p=7309262&hil ... e#p7309262
DSP-AR-20005
User avatar
skow69
Site Donor
Site Donor
Posts: 3230
Joined: Tue Dec 06, 2011 3:03 am
Location: Cascadia

Re: Vapor management take off rates question

Post by skow69 »

+1.
You're still at 4:1 reflux ratio. Hence no improvement.

It wouldn't be hard to chuck the valve and make a slideable coil. Stay 2" to the elbow. Probably get 1/2 gallon per hour.
Distilling at 110f and 75 torr.
I'm not an absinthe snob, I'm The Absinthe Nazi. "NO ABSINTHE FOR YOU!"
rad14701
retired
Posts: 20865
Joined: Wed Dec 19, 2007 4:46 pm
Location: New York, USA

Re: Vapor management take off rates question

Post by rad14701 »

Marbles may or may not work well in your modified column but nothing venture, nothing gained... Marbles are fairly inexpensive and can be used for decoration when no in use... My extras are in a fancy wire basket on the entertainment center in the living room...
copperlover1
Swill Maker
Posts: 250
Joined: Mon Jan 06, 2014 8:59 am

Re: Vapor management take off rates question

Post by copperlover1 »

Going with the 2" take off. 2" elbow. Easy flange to my old condenser. I will have to get some ss gas line to make the adjustable condenser.
Attachments
image.jpg
hellbilly007
Site Donor
Site Donor
Posts: 582
Joined: Fri Aug 03, 2012 10:59 am
Location: Never one place very long

Re: Vapor management take off rates question

Post by hellbilly007 »

Damn you move quick, lol. That's a nice shotgun condenser, :thumbup: If you wish, you can use a 2" to 1/2" as opposed to the 2" to 1" you mention in your pic, it will make the output stream easier to direct. If you already have the reducer you've mentioned disregard that last sentence. Your ambition is making me feel like a major slacker here.
copperlover1
Swill Maker
Posts: 250
Joined: Mon Jan 06, 2014 8:59 am

Re: Vapor management take off rates question

Post by copperlover1 »

All soldered up and ready for the next step. Reflux condenser. Going with ss flex gas line.
Attachments
image.jpg
Post Reply