Clearing sugar wash - any tips and tricks?
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Clearing sugar wash - any tips and tricks?
hi All
I’m in a bit of a hurry and cannot wait 2 weeks for the wash to settle. As the wash is 100 liters, I cannot move it outside - a cold crash would work best
the temperature is 20 C where the fermentor is places - so what will work here?
I’m in a bit of a hurry and cannot wait 2 weeks for the wash to settle. As the wash is 100 liters, I cannot move it outside - a cold crash would work best
the temperature is 20 C where the fermentor is places - so what will work here?
- still_stirrin
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Re: Clearing sugar wash - any tips and tricks?
Steam. If you have the right equipment any situation can be overcome.
Where’s the fire?
ss
My LM/VM & Potstill: My build thread
My Cadco hotplate modification thread: Hotplate Build
My stock pot gin still: stock pot potstill
My 5-grain Bourbon recipe: Special K
My Cadco hotplate modification thread: Hotplate Build
My stock pot gin still: stock pot potstill
My 5-grain Bourbon recipe: Special K
Re: Clearing sugar wash - any tips and tricks?
Is this for the commercial distillery mentioned in your "hello" thread?
What size still?
Electric, steam or electric element?
Can you run dirty or must it be clean?
Can you not move that by way of 5 or 6 buckets outside to cold crash it if that is what you want to do?
Any pumps and hoses?
What are you using sugar washes for if for commercial use? Is grains not cheaper to mash from and produce better spirits?
What's the current SG of the wash?
What size still?
Electric, steam or electric element?
Can you run dirty or must it be clean?
Can you not move that by way of 5 or 6 buckets outside to cold crash it if that is what you want to do?
Any pumps and hoses?
What are you using sugar washes for if for commercial use? Is grains not cheaper to mash from and produce better spirits?
What's the current SG of the wash?
Programmer specializing in process control for ExxonMobil (ethanol refinery control), WT, Omron, Bosch, Honeywell & Boeing.
More than a decade working for NASA & FAA Tech with computer code used on Space Shuttles and some airline flight recorders.
More than a decade working for NASA & FAA Tech with computer code used on Space Shuttles and some airline flight recorders.
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Re: Clearing sugar wash - any tips and tricks?
Yah.. where's the fire..
If you really want to clear that sugar wash in a few days.. it needs to be racked off its lee, and I mean rack and not siphon.. then once it's transfer to another holder, degas it well by giving a good stir with a drill and stirer, then you can add a 2 part clarifier and it should clear within 4 -5 days..
Mars
" I know quite certainly that I myself have no special talent. Curiosity, Obsession and dogged endurance, combined with self-criticism, have brought me to my knowledge and understanding "
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Re: Clearing sugar wash - any tips and tricks?
If we knew what sort of sugar wash it was we might be able say if it really needs clearing or not. There is every chance you don't need it perfectly clear prior to stripping.
Re: Clearing sugar wash - any tips and tricks?
Hi all
Sadly we cannot move it outside, as it's not permitted where we are - we are hoping to move soon, but then what in the summer if we need a bit of holiday ?
The SG is now 1.020 and very soon ready to be distilled. About a week ago I ran a batch that had not settled and even though the product taste like heaven, there is a small smell of yeast ( not a pleasant smell )
These batches are only for us - trying to have a good base to make "snaps " for the Christmas dinners in our families and with friends
The still i'm using for these small batches is a 100 liters 4 plate still with a heat element inside.
Is is possible to use gelatin or simialr to catch the yeast and force them down ?
Sadly we cannot move it outside, as it's not permitted where we are - we are hoping to move soon, but then what in the summer if we need a bit of holiday ?
The SG is now 1.020 and very soon ready to be distilled. About a week ago I ran a batch that had not settled and even though the product taste like heaven, there is a small smell of yeast ( not a pleasant smell )
These batches are only for us - trying to have a good base to make "snaps " for the Christmas dinners in our families and with friends
The still i'm using for these small batches is a 100 liters 4 plate still with a heat element inside.
Is is possible to use gelatin or simialr to catch the yeast and force them down ?
Re: Clearing sugar wash - any tips and tricks?
Sorry CaperH, I misunderstood your first post and thought you were asking how to move it outside since you "can't do it".
Got it "not allowed" to do it so looking for other methods.
I'd say since the SG is still 1.020 (pretty high) and this is a sugar wash it's not done fermenting yet let alone cleared. You still have another 2.6%+ potential ABV left in the wash to ferment which is a decent amount.
I'd be more worried about running this with all that sugar left in the batch then the yeast as far as taste goes.
You need to give it TIME to properly finish fermenting and then a bit of time (if you want) to settle.
Got it "not allowed" to do it so looking for other methods.
I'd say since the SG is still 1.020 (pretty high) and this is a sugar wash it's not done fermenting yet let alone cleared. You still have another 2.6%+ potential ABV left in the wash to ferment which is a decent amount.
I'd be more worried about running this with all that sugar left in the batch then the yeast as far as taste goes.
You need to give it TIME to properly finish fermenting and then a bit of time (if you want) to settle.
Programmer specializing in process control for ExxonMobil (ethanol refinery control), WT, Omron, Bosch, Honeywell & Boeing.
More than a decade working for NASA & FAA Tech with computer code used on Space Shuttles and some airline flight recorders.
More than a decade working for NASA & FAA Tech with computer code used on Space Shuttles and some airline flight recorders.
- still_stirrin
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Re: Clearing sugar wash - any tips and tricks?
Try it...you’re commercial, right?
Obviously you have a working knowledge of processes and tools available to produce your products. It would appear that you’re seeking a solution here to resolve your urgency. So, if you want to run it early...run it. If you want to fine/clarify it, then do it. You don’t need approval from this site how to produce your (commercial) product. Use your experience and just do it.
If this is too succinct, sorry...you’re not a novice. You’re a commercial producer. You should know what to do already.
ss
My LM/VM & Potstill: My build thread
My Cadco hotplate modification thread: Hotplate Build
My stock pot gin still: stock pot potstill
My 5-grain Bourbon recipe: Special K
My Cadco hotplate modification thread: Hotplate Build
My stock pot gin still: stock pot potstill
My 5-grain Bourbon recipe: Special K
Re: Clearing sugar wash - any tips and tricks?
We are very small and in some ways novices and in others not
Vodka I can make, some gin - but thats about it. We do have a bit of commercial stuff, but it's not our day job - we all have very normal very boring jobs. It started out with a hobby that grew, when a friend of ours called ud: Hey guys, we have 300 events a year and we need vodka, we need a bit of gin and we need alot of those " shots " we like - you know - those sour strawberry shots, that mango peach shot and those damn good liquorice shots!
So I do feel more like a chef than a distiller - as I mostly do neutral and mix it with extract made in the kitchen - but it's very fun.
And we are no way close to going solo - taxes on spirits are crazy, rent is insane and prices are low. But that is ok, as we want to learn, we want to explore and most of all - we just want sit on a friday evening and enjoy something we made by our own hands.
Anyways - Normally i let it ferment dry and then let it rest - if possible cold crash it.
But as Christmas is comming fast and if we are going to be serving nice x-mas snaps, green walnut snaps and other fun things - at the traditional christmas lunches - I kinda need some neutral as soon as it fermented dry.
The family have been looking at my walnut solution for 2 years now and I promised a taste this year - and now I'm out of neutral. Oh boy!
So if anyone have a good idea please share - i'm sure it would be good info for others at the forum
Vodka I can make, some gin - but thats about it. We do have a bit of commercial stuff, but it's not our day job - we all have very normal very boring jobs. It started out with a hobby that grew, when a friend of ours called ud: Hey guys, we have 300 events a year and we need vodka, we need a bit of gin and we need alot of those " shots " we like - you know - those sour strawberry shots, that mango peach shot and those damn good liquorice shots!
So I do feel more like a chef than a distiller - as I mostly do neutral and mix it with extract made in the kitchen - but it's very fun.
And we are no way close to going solo - taxes on spirits are crazy, rent is insane and prices are low. But that is ok, as we want to learn, we want to explore and most of all - we just want sit on a friday evening and enjoy something we made by our own hands.
Anyways - Normally i let it ferment dry and then let it rest - if possible cold crash it.
But as Christmas is comming fast and if we are going to be serving nice x-mas snaps, green walnut snaps and other fun things - at the traditional christmas lunches - I kinda need some neutral as soon as it fermented dry.
The family have been looking at my walnut solution for 2 years now and I promised a taste this year - and now I'm out of neutral. Oh boy!
So if anyone have a good idea please share - i'm sure it would be good info for others at the forum
Re: Clearing sugar wash - any tips and tricks?
You may have been sold unrealistic expectations of what your plater is capable of, in which case, spending a lot of effort to clear the wash might not give you the improvement you are hoping for. Stripping the wash with a pot still before it goes into a plater works well, but you still have to get the cuts right.
Re: Clearing sugar wash - any tips and tricks?
What does cold crash mean and how do you do it?
Re: Clearing sugar wash - any tips and tricks?
Cold crashing is a simple process of exposing your ferment (when done) to cold temps. You could rack to 5 or 6 gallon carboys and place it outside in the winter or a refrigerator. The cold (not freezing) temps help the wash to settle much faster. As just an example what could take 2 or 3 days to settle on it's own might take 1 or 2 hows when cold crashed. If freezing out just moderate it from outside to inside in 30 or 60 minute increments (ie inside the door to outside the door).
If you set it outside in freezing weather then you'll end up doing freeze distillation where the water will freeze put not the alcohol, so if this happens by accident just flip the container and drain into another container. The ice and trub will be frozen so just watch when pouring back out and stop the pour when only the trub and water is left (will be lots of ice crystals). This will concentrate the alcohol and flavors. 8% mash will end up 15 to 20% after one freeze distillation, maybe up to 25% after a second freeze distillation, etc... I will sometimes do this on purpose in the winter for some spirits to concentrate flavor and ABV and do this instead of strip runs to save time.
But cold crashing is just using cold temps above freezing to get the yeast and other particles to settle much faster.
If you set it outside in freezing weather then you'll end up doing freeze distillation where the water will freeze put not the alcohol, so if this happens by accident just flip the container and drain into another container. The ice and trub will be frozen so just watch when pouring back out and stop the pour when only the trub and water is left (will be lots of ice crystals). This will concentrate the alcohol and flavors. 8% mash will end up 15 to 20% after one freeze distillation, maybe up to 25% after a second freeze distillation, etc... I will sometimes do this on purpose in the winter for some spirits to concentrate flavor and ABV and do this instead of strip runs to save time.
But cold crashing is just using cold temps above freezing to get the yeast and other particles to settle much faster.
Programmer specializing in process control for ExxonMobil (ethanol refinery control), WT, Omron, Bosch, Honeywell & Boeing.
More than a decade working for NASA & FAA Tech with computer code used on Space Shuttles and some airline flight recorders.
More than a decade working for NASA & FAA Tech with computer code used on Space Shuttles and some airline flight recorders.
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Re: Clearing sugar wash - any tips and tricks?
What's the difference between racking and siphon?StillerBoy wrote: ↑Sun Dec 08, 2019 3:23 pmYah.. where's the fire..
If you really want to clear that sugar wash in a few days.. it needs to be racked off its lee, and I mean rack and not siphon.. then once it's transfer to another holder, degas it well by giving a good stir with a drill and stirer, then you can add a 2 part clarifier and it should clear within 4 -5 days..
Mars
Re: Clearing sugar wash - any tips and tricks?
That's a good question. Siphoning is just a typical method of doing the racking from one container to another leaving the trub/lees behind.
Mars, care to clarify what you meant?
Mars, care to clarify what you meant?
Programmer specializing in process control for ExxonMobil (ethanol refinery control), WT, Omron, Bosch, Honeywell & Boeing.
More than a decade working for NASA & FAA Tech with computer code used on Space Shuttles and some airline flight recorders.
More than a decade working for NASA & FAA Tech with computer code used on Space Shuttles and some airline flight recorders.
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Re: Clearing sugar wash - any tips and tricks?
Yeah I thought rack and siphon were the same thing...
Though there may be an implication in the word 'rack' that you draw from clear of the sediment.
Which I would do anyway...
Geoff
Though there may be an implication in the word 'rack' that you draw from clear of the sediment.
Which I would do anyway...
Geoff
The Baker
Re: Clearing sugar wash - any tips and tricks?
I'd consider racking the overall separation of the liquid from the lees/trub. This could be moving the liquid leaving just the lees/trub behind using a bucket, cup, pump, siphon, etc OR if using a conical style fermenter the opposite is done where you open a valve slowly at the bottom and drain off the les/trub leaving just the clear liquid.
I was just wondering what Mars was getting at my making the distinction the way he did.
I was just wondering what Mars was getting at my making the distinction the way he did.
Programmer specializing in process control for ExxonMobil (ethanol refinery control), WT, Omron, Bosch, Honeywell & Boeing.
More than a decade working for NASA & FAA Tech with computer code used on Space Shuttles and some airline flight recorders.
More than a decade working for NASA & FAA Tech with computer code used on Space Shuttles and some airline flight recorders.
Re: Clearing sugar wash - any tips and tricks?
Just curious as to what type of a fermenter you use. I have a few 6 gallon food grade buckets.cayars wrote: ↑Sun Feb 02, 2020 12:43 pm I'd consider racking the overall separation of the liquid from the lees/trub. This could be moving the liquid leaving just the lees/trub behind using a bucket, cup, pump, siphon, etc OR if using a conical style fermenter the opposite is done where you open a valve slowly at the bottom and drain off the les/trub leaving just the clear liquid.
I was just wondering what Mars was getting at my making the distinction the way he did.
I don't drink alcohol, I drink distilled spirits.
Therefore I'm not a alcoholic, I'm spiritual.
Therefore I'm not a alcoholic, I'm spiritual.
Re: Clearing sugar wash - any tips and tricks?
I've got a few different things I use.
2 - 7.9 gallon conical fermenters I use mainly for wines/brandy but if not making wine will likely have malted barley (off grain) in them for making scotch. These have a drain valve at the bottom and I've got them mounted on the wall. So these you "rack" by removing the crud and leaving the liquid. NICE
2 - 44 Gallon & 1 - 32 Gallon Brute trashcans for open top ferments. I have these on wheels so I can move them around. These I use for different whiskeys or my vodka ferments. I've got a ball valve at 6" and also at about 18" marks on these. So if fermenting off grain I can drain using the lowest valve and if on grain can use the higher valve to drain off the clear liquid, then pull off the dirty for putting in a thumper or cold chilling.
A bunch of 5 gallon plastic water carboys and home depot/lowes buckets - Typically I use these only for non grain stuff like Rums or neutral sugar wash mashes. These all have airlocks like the conical fermenters. I also use these when "racking" from the brutes or to cold chill in or to use to fill boilers.
So I can sort of juggle what goes where based on what I'm making.
I'm likely to try and retire the brutes this spring summer and replace them with 55 gallon plastic barrels you can usually find cheap. I want the sealed ones so I can get away from open top ferments. I had a tough time with fruit flys this past year. Those are some nasty little suckers!
My basement temps run 65F to 80F (winter to summer) so a different choice of yeast solves any temp issues.
I'd really love to have a bunch of bigger conical fermenters but they get pricey. Come spring I'll be ramping things up across the board since I'll be able to process a lot more spirits with the newer system I'm building with 26 gallon boiler and keg thumpers for stripping. I should be able to process a brute trashcan ferment in one stripping run. The 3 brutes will give me 3 strip runs then 1 spirit run. I've had to do some rewiring for electric. Tired of running the bigger keg still in the garage using propane (to hot or cold most of the time and no water supply, tv or internet). This is going to be a "automated" still when I get done with it similar to an iStill or Genio. I've got multiple stills so I will be able to run a couple at the same time as well. Most likely stripping on one and spirit runs on the other or heating water while running one still, etc
2 - 7.9 gallon conical fermenters I use mainly for wines/brandy but if not making wine will likely have malted barley (off grain) in them for making scotch. These have a drain valve at the bottom and I've got them mounted on the wall. So these you "rack" by removing the crud and leaving the liquid. NICE
2 - 44 Gallon & 1 - 32 Gallon Brute trashcans for open top ferments. I have these on wheels so I can move them around. These I use for different whiskeys or my vodka ferments. I've got a ball valve at 6" and also at about 18" marks on these. So if fermenting off grain I can drain using the lowest valve and if on grain can use the higher valve to drain off the clear liquid, then pull off the dirty for putting in a thumper or cold chilling.
A bunch of 5 gallon plastic water carboys and home depot/lowes buckets - Typically I use these only for non grain stuff like Rums or neutral sugar wash mashes. These all have airlocks like the conical fermenters. I also use these when "racking" from the brutes or to cold chill in or to use to fill boilers.
So I can sort of juggle what goes where based on what I'm making.
I'm likely to try and retire the brutes this spring summer and replace them with 55 gallon plastic barrels you can usually find cheap. I want the sealed ones so I can get away from open top ferments. I had a tough time with fruit flys this past year. Those are some nasty little suckers!
My basement temps run 65F to 80F (winter to summer) so a different choice of yeast solves any temp issues.
I'd really love to have a bunch of bigger conical fermenters but they get pricey. Come spring I'll be ramping things up across the board since I'll be able to process a lot more spirits with the newer system I'm building with 26 gallon boiler and keg thumpers for stripping. I should be able to process a brute trashcan ferment in one stripping run. The 3 brutes will give me 3 strip runs then 1 spirit run. I've had to do some rewiring for electric. Tired of running the bigger keg still in the garage using propane (to hot or cold most of the time and no water supply, tv or internet). This is going to be a "automated" still when I get done with it similar to an iStill or Genio. I've got multiple stills so I will be able to run a couple at the same time as well. Most likely stripping on one and spirit runs on the other or heating water while running one still, etc
Programmer specializing in process control for ExxonMobil (ethanol refinery control), WT, Omron, Bosch, Honeywell & Boeing.
More than a decade working for NASA & FAA Tech with computer code used on Space Shuttles and some airline flight recorders.
More than a decade working for NASA & FAA Tech with computer code used on Space Shuttles and some airline flight recorders.
Re: Clearing sugar wash - any tips and tricks?
Bentonite of course.
Dissolve 80 grams (for 100 liters of wash) of it in warm water, add to the wash and stir well. Wash will clear in a couple of days. No after-taste or whatsoever. Actually it will taste better after bentonite as the sediments in the wash settle down.
Re: Clearing sugar wash - any tips and tricks?
Clearing the wash:
Time - particulates will naturally settle out over time but this is long and doesn't control fermentation
Cold crash - chill the wash to 1-2C and let the particulates settle rapidly. A 10% wash will freeze at -4C so be careful of temps <0C since ice crystals will start to form around the sides. The wash won't partially freeze because ethanol emulsifies excellently with water. This also stops the ferment in its tracks
Bentonite / Turbo Clear (kieselsol) / gelatine - benefit here is it doesn't require energy to chill and it's just as quick as cold crashing. Need to degas your wash (use a drill, vacuum pump, or chitosan (which is part A of the Turbo Clear pack)). Stir the bentonite / kieselsol (part B of the Turbo Clear pack) / gelatine around the top layer only and not through the mix. Gravity will pull this layer down through the wash, capture the particulates, and settle them to the bottom. Note that gelatine will absorb a lot more of the wash.
Mechanical filter - depending on your membrane pores, you can pump the wash through a mechanical filter to clarify it. Since the particle sizes vary greatly, would recommend a multi-stage filter system for this. Otherwise you could pretty easily clog up a filter membrane
Time - particulates will naturally settle out over time but this is long and doesn't control fermentation
Cold crash - chill the wash to 1-2C and let the particulates settle rapidly. A 10% wash will freeze at -4C so be careful of temps <0C since ice crystals will start to form around the sides. The wash won't partially freeze because ethanol emulsifies excellently with water. This also stops the ferment in its tracks
Bentonite / Turbo Clear (kieselsol) / gelatine - benefit here is it doesn't require energy to chill and it's just as quick as cold crashing. Need to degas your wash (use a drill, vacuum pump, or chitosan (which is part A of the Turbo Clear pack)). Stir the bentonite / kieselsol (part B of the Turbo Clear pack) / gelatine around the top layer only and not through the mix. Gravity will pull this layer down through the wash, capture the particulates, and settle them to the bottom. Note that gelatine will absorb a lot more of the wash.
Mechanical filter - depending on your membrane pores, you can pump the wash through a mechanical filter to clarify it. Since the particle sizes vary greatly, would recommend a multi-stage filter system for this. Otherwise you could pretty easily clog up a filter membrane