ultrasonic aging experiment

Any hardware used for mashing, fermenting or aging.

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SaltyStaves
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Re: ultrasonic aging experiment

Post by SaltyStaves »

DBCFlash wrote: To be fair, I will consider running a session with an oak block from start to finish, but I am really skeptical about it's value. I am going to wait until I have installed a cooling fan though, since I believe it will draw a lot more energy and probably create more heat in the controller.
When you do run the test, it may also be a good idea to run an identical control test with passive oaking and maybe also a test with the same distillate pretreated with US and then oaked. Then come back to all three of them several months down the line. This should give you an idea if there is any merit in one treatment over the other.

The thing with disruptive processes like US, is that its similar to the distillation process and it breaks things at the molecular level. With time/aging/ripening in the jar, things will settle/marry and change and that can be good or bad. It really depends on your end goal and how quickly you intend to consume it, but if my goal was to pretreat with US and then long term age, I'd want to be sure that I wasn't cleaning up something that could lead to drinkable New Make now, at the cost of boring brown spirit months/years later.
But half the fun is finding out.

I'm watching with interest. :thumbup:
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skow69
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Re: ultrasonic aging experiment

Post by skow69 »

DBCFlash wrote: The second part was the application of "actinic light" with the charred wood chips. Actinic light, as I understand it are specific blue end wavelengths that are used for photosynthesis. They appear to be using some pretty powerful actinic lights to get the reaction from the oak.
Actually plants use mainly red wavelengths for photosynthesis. They appear to be green because they reflect that and absorb the red. If anything, blues would probably inhibit photosynthesis. Also IIRC ultraviolet leds often come with warnings to avoid exposure, like they are not beneficial to human health.
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Re: ultrasonic aging experiment

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skow69 wrote: Actually plants use mainly red wavelengths for photosynthesis. They appear to be green because they reflect that and absorb the red. If anything, blues would probably inhibit photosynthesis. Also IIRC ultraviolet leds often come with warnings to avoid exposure, like they are not beneficial to human health.
You won't find many marine aquariums with red lights. Coral need to photosynthesize and they have more in common with a submerged piece of wood than a leaf on a tree.
This is fairly off topic, so I'll leave it at that.
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skow69
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Re: ultrasonic aging experiment

Post by skow69 »

Since we don't have any red oceans, fish tanks are probably more attractive in green. But nobody is photosynthesizing green light.
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DBCFlash
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Re: ultrasonic aging experiment

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skow69 wrote:
DBCFlash wrote: The second part was the application of "actinic light" with the charred wood chips. Actinic light, as I understand it are specific blue end wavelengths that are used for photosynthesis. They appear to be using some pretty powerful actinic lights to get the reaction from the oak.
Actually plants use mainly red wavelengths for photosynthesis. They appear to be green because they reflect that and absorb the red. If anything, blues would probably inhibit photosynthesis. Also IIRC ultraviolet leds often come with warnings to avoid exposure, like they are not beneficial to human health.
Investigate actinism.
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contrahead
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Re: ultrasonic aging experiment

Post by contrahead »

I've been offline for a week; because of router problems, family medical appointments and attendance to the needs of visiting guest. Finally fixed the Internet connection problem after crawling around on my hands an knees in search for cat-V cable or DSL phone line issues.

I wish to address a few statements or ideas from “DBCFlash”. (where he said)

-“I would compare the change to be like a pot of chili......1st day you can find or taste each individual ingredient …...but next day the flavors have merged”....
-“I will continue to set aside a dram of untreated each time to make comparisons”
-“the presence of the oak block might interfere with the wave propagation. It's porous nature would likely just absorb the energy”
-“the microscopic cloud of bubbles immediately stopped practically the moment the wood was introduced”

Firstly, the analogy between aging spirits and the seasonings melding in chili - is a very good one.
Secondly, I wonder how many people here recognize how small a dram really is? I've only seen the word used probably on the side of boxes of shotgun shells where “dram equivalent” is supposed to indicate how much recoil is to be expected. (When black powder was the primary propellant in shotguns it was measured in drams ( 1⁄256 pound or  1⁄16 ounce )). Today's US teaspoon is equivalent to exactly  1⁄6 US fluid ounces or  1 1⁄3 US fluid drams. A “shot” is legally defined in the U.S. as having one fluid ounce in volume. The 1.5 oz “jigger” was adopted by bartenders because the “official shot” made for a stingy drink. It would take 8 drams to fill a legal shot glass or 12 drams to fill a normal jigger.

Finally, wood is very porous and probably does act like a big sponge that absorbs energy, but; perhaps you are not using enough energy. After watching several videos on ultrasonic cleaning I noticed that several setups used multiple transducers and multiple frequencies to clean items. Cavitation alone without wood chips probably benefits new-make spirit. Upping the amplification of the acoustic energy delivered seems necessary to overcome the loss absorbed by added wood.

I am hesitant to speculate how far or how fast the spirit soaks into dry wood chips, and then what might be happening at the molecular level if vapor cavities begin to form on the surface or below the surface of that wood. Also: the bubbles from boiling and the “bubbles” from cavitation are very different. During a boil, gas in solution within the liquid is released and since it is lighter than the liquid – it will rise to the surface. Bubbles caused by cavitation however are voids or vacuums caused by the liquid being pulled. These type of bubbles contain no gas or vapor. While these short -lived bubbles might not be compelled to rise they can implode vigorously instead – creating those intense little shock waves that are substantial enough to eat metal away from propellers, turbine rotors and pumps.
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Re: ultrasonic aging experiment

Post by DBCFlash »

In this case, a "dram" represents an unmeasured, small quantity of spirits, maybe half a shot or so. Enough to have a decent taste or three.

My UAD is no longer functional. I built a nice case for it, wired in a digital timer and a cooling fan and once it was all back together, it didn't work. I've been trouble-shooting it and it looks like my transistors are blown. I'll probably order a new board, but I also might try just replacing the transistors. I knew this device was a delicate little flower, but this is just stupid.
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Re: ultrasonic aging experiment

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Talked to a friend who is working with some electrical engineering grad students and I might be getting some help replacing my ultrasonic driver with something more robust.
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Re: ultrasonic aging experiment

Post by contrahead »

An old foreman used the expression “I'm busier than a cat covering up shit”. It kind of fits my situation at the moment.

The fermentation bucket works almost every day of the year, the still every couple of weeks. But for the time being and until the weather changes, experimentation will have to take a back seat to water-sports, outdoor construction projects and travel.
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Re: ultrasonic aging experiment

Post by contrahead »

Thought I'd drop a newfound link in this thread, to an informative blog about ultrasonic cleaning. The blog is not organized like a book but can be searched by category or keyword. There are short multiple or weekly installments for each month in the archives. A few examples follow.

http://techblog.ctgclean.com/2012/01/ul ... what-is-q/" onclick="window.open(this.href);return false;" rel="nofollow

http://techblog.ctgclean.com/2012/01/ul ... -hardware/" onclick="window.open(this.href);return false;" rel="nofollow

http://techblog.ctgclean.com/2011/11/ul ... implosion/" onclick="window.open(this.href);return false;" rel="nofollow

http://ctgclean.wpengine.com/wp-content ... ng-LD1.wmv" onclick="window.open(this.href);return false;" rel="nofollow
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Re: ultrasonic aging experiment

Post by markx »

I have been experimenting with the ultrasound ageing technique lately and from what I've seen so far working with rather old (10+ years cask aged) rye whisky I could summarize as following:
1) Subjecting the drink to ultrasonic treatment really does alter its character. The changes are not too subtle and extend into all characteristics of the product as far as smell, taste and coloration are concerned.
2) The effect of ultrasound is in strong conjunction with the effect of surrounding atmosphere. Subjecting the drink to aeration after or before ultrasonic treatment produces totally different characteristics.
3) The effect of rapid characteristics change initiated by the ultrasonic treatment extends over a month after the actual treatment has been performed.
4) To get strongly noticeable effects the ultrasonic treatment has to be run continuously for at least 5 days.
5) When used in conjunction with aeration the treatment can either improve or worsen the characteristics of the drink depending in which order the operations are performed. Namely subjecting the drink to aeration before ultrasonic ageing seems to harshen the taste and make the drink actually appear younger than before the treatment. Doing it in reverse order: aerating after ultrasonic treatment seems to favor the formation of a smooth well aged taste and a noticeable darkening of color.

I have so far performed 2 blind tasting sessions with the resulting beverages from three different treatment regimes and stemming from one source of whisky:

a) Untreated 10+ years cask aged rye whisky as the control
b) 10+ years cask aged rye whisky treated with ultrasound for 5 days in a closed glass bottle
c) result from previous treatment subjected to mild aeration with a wooden air stone and aquarium pump for 12h
d) 10+ years cask aged whisky subjected to mild aeration for 12h and then treated with ultrasound for 5 days

Ultrasonic treatment was performed in glass vessels with a RETCH UR1 cleaner unit in continuous operation mode at 55C temperature. The temperature arose from just the heat of the transducer losses in the bath and no external heating was applied. Aeration was carried out at 19-20C through a miniature wooden air stone and propelled by an aquarium air pump. The amount of air going through the samples was not monitored, but it was mild enough to not change the alcohol content appreciably during the 12h cycle.

The tasting results were as following:
Sample a) : Rather mediocre in all aspects, some rugged edges in the taste profile despite the rather long maturation period. Drinkable, but not going to win any prizes.
Sample b) : Appreciably milder than the control sample, more rounded taste profile, noticeable vanilla and caramel tones arising in the aroma, ever so slightly darker than control sample.
Sample c) : Much darker in coloration than the first two samples, wonderful caramel and vanilla like aroma, almost perfectly smooth taste without any rugged notes of the original control sample, definitely the best of the four samples.
Sample d) : Almost as dark as the sample c, aroma profile also very similar to sample c, but perhaps a bit less intense, taste very much degraded with a profound sharpness and totally opposite to previous sample. It seemed much younger than even the control sample with profound sharp extending notes and a very bad burn that slowly built up in throat after tasting.

None of the participants could believe that all the samples stemmed from the same source. The taste and smell characteristics were too different at first glance.


Perhaps not as scientific as one could desire, but there seems to be quite a lot going on around the ultrasonic treatment technique. Definitely worthwhile to investigate more deeply and especially in conjunction with aeration, as this proved to enhance the effects under certain conditions. What is also noticeable is the fact that the processes initiated by the treatments seemed to go on in closed bottles quite intensively for over a month afterwards. The taste and aroma profiles continued to quickly develop for all samples and then seemed to run into a plateau. Interestingly sample d did not improve much and despite a rather nice aroma it remained quite harsh, as if all the previous ageing had been undone for the part of taste...
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Re: ultrasonic aging experiment

Post by Bushman »

Most use ultra sonic aging as a kickstart on newly distilled products. I have no data but would not think it would enhance a product that has been aged for 10 years. Sounds like you have well documented your tests!
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Re: ultrasonic aging experiment

Post by markx »

Bushman wrote:Most use ultra sonic aging as a kickstart on newly distilled products. I have no data but would not think it would enhance a product that has been aged for 10 years. Sounds like you have well documented your tests!
As my mother always told me: "One must always try new things" :D But jokes aside...the vibrations actually play quite some tricks on the aged spirits. I must admit that I have not yet tried it on newly distilled spirits, but I am sure that there will be some effects. The patterns for obtaining best results may of course differ from the ones that apply to the aged stuff, but time will tell.
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Re: ultrasonic aging experiment

Post by jonnys_spirit »

What was the frequency of the ultrasound and is it possible to modulate the frequency or amplitude with another audio signal? Ie; music...

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Re: ultrasonic aging experiment

Post by markx »

jonnys_spirit wrote:What was the frequency of the ultrasound and is it possible to modulate the frequency or amplitude with another audio signal? Ie; music...

Cheers!
-j
Please find the respective data in the link below:

https://www.retsch.com/products/assisti ... -features/

There is no option to regulate output power or characteristics on the UR1 unit....it just blasts with full power in continuous mode at 38kHz which is one of the standard oscillating ranges for transducers.
As for modulating the signal, it can be done if one custom builds the driver hardware in the appropriate way, but it is complicated and energetic losses would be big for frequency modulation. The transducers exhibit a certain selfoscillation frequency and the drive circuit and tank/horn assembly is tuned closely into that specific frequency to obtain resonance and hence a high efficiency. It must be noted that the selfoscillation frequency is highly dependant on many factors (basically every piece of equipment in physical contact with the transducer will shift the frequency). Long story short....it is quite difficult to tune a ultrasonic generator to high output efficiency and one has to be well versed in the science behind it to achieve a satisfactory result. Just taking a transducer, gluing it to the bottom of a bowl and connecting a generic drive circuit will rarely produce anything good. I tried it myself, but found that it is way easier to use a commercial high efficiency unit than trying to craft something on your own.
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Re: ultrasonic aging experiment

Post by dr_canak »

I know there are several posts here, but this seems to be one of the more recently active ones...

I purchased an "Alpine 1 Jet Fogger with Transformer" from Amazon for $25.00. The kind of little US device that is made for tabletop fountains. I put 750mls (65F) of a neutral sugarwash (33% ABV) that I just ran last week into a 1l glass beaker. The wash is a mashup of some recipes here, and run through a T-500.

Dropped in the US fogger, plugged it in, and ran it for 10 minutes. There was a marked difference between the artificially "aged" spirit and the non-aged spirit. The US "aged" spirit was definitely less harsh and had lost most of the "burn" associated with my neutrals. I liked them both equally well, but to someone unaccustomed to a sugar wash shine, I would imagine the US "aged" spirit will almost certainly be favored.

Obviously, doing this 1l at a time, with my little fogger, isn't all that efficient. But it was an inexpensive opportunity to start experimenting. ymmv.
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Re: ultrasonic aging experiment

Post by chickenfeed »

Ok, I am going to build on of these for myself. I got this off Amazon 60W 40KHz Ultrasonic Cleaning Transducer Cleaner + Power Driver Board 110V AC $36.99 Plan on using a stainless steel 20quart stock pot for the container. I have ujssm THAT IS 8 MONTHS ON oak and has all the oak i want but still tastes a little sharp. I will let ou all know the results but for the price I have to do it. a gallon sonic cleaner os about 450 500$$
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Re: ultrasonic aging experiment

Post by raketemensch »

I wonder how people are tasting these for comparisons.

The second sip of any hard liquor is going to seem less harsh, that’s just the nature of human tissue.
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Re: ultrasonic aging experiment

Post by chickenfeed »

Ok the results are in. It’s no substitute for a year in a 5gal barrel but when I oak it in glass until I get the color and taste I want then 4 four hour sessions in the rig and it’s very smooth.
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Re: ultrasonic aging experiment

Post by Bushman »

chickenfeed wrote:Ok the results are in. It’s no substitute for a year in a 5gal barrel but when I oak it in glass until I get the color and taste I want then 4 four hour sessions in the rig and it’s very smooth.
This is basically what most of us have concluded. It’s a nice start to give you an idea but it is not a full substitute. Adds more color than age.
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Re: ultrasonic aging experiment

Post by Zxlork »

I know I'm a little late to the party...but going to be doing some tests in regards to the US aging this fall in regards to the proper wavelength for oak. Apparently, according to the russians, there are certain wavelengths that actually resonate with each wood species which in turn would mean using the right frequency with the right wood would make the wood resonate with the frequency thus increasing its effectiveness.

https://www.semanticscholar.org/paper/E ... -Resonant-(RUS" onclick="window.open(this.href);return false;" rel="nofollow)%3A-Longo-Laux/c5ecb125a243bdd0ac6822ed5ac83593d4afff32
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Re: ultrasonic aging experiment

Post by Bushman »

Have not heard it was that specific. For most of us with US cleaners we can not control the frequency but temps. I am guessing you would be talking about a very specific and expensive piece of equipment.
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Re: ultrasonic aging experiment

Post by Zxlork »

Yes and no. Yes as in might be if you can not find the resonance frequency of oak in a research paper(still doing more research). Once that is ascertained it's as simple as getting/making something for this frequency range and anyone here could use it. Mainly because most people use oak...but different kinds of oaks would obviously have slightly different resonance. My hope is that Oak as a species has a close frequency range...so regardless of what you do it would work but only time/research will tell.
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