Micro Still 9 Litre Wonder

Simple pot still distillation and construction with or without a thumper.

Moderator: Site Moderator

Post Reply
zwinzilious
Novice
Posts: 20
Joined: Tue Jul 20, 2010 3:26 am

Micro Still 9 Litre Wonder

Post by zwinzilious »

Hi all,

Glad to have started this journey. The truth is, I have had visions of doing this for a long time. Glad the process of actually doing it, was easier than what conventions will have us believe.

So can a still be made, constructed, as well as produce a quality spirit hygienically, safely, with limited resources, tools, and your friendly European Ikea store in a European country-? Sure, and I may publish just how easy. For starters you can pick up a 9 litre stock pot from Ikea for about 25 Euros, stainless steel, and with nice handles for "Handling".

Next you need your worm, your holding container filled with cool water and ice blocks from a freezer. The worm is another 20 Euros. You then need your connection parts, and 2 holes in the top of your IKEA stock pot. Also, you can pick up your nice perfect digital Ikea heat thermometer 9 Euros. (Second hole in lid is to seat a fitting and a cork, fixed with your thermometer. When the basic Pot still is all soldered with silver solder, clamps, you can now find your fermenter, which is simple in my european country, because 15L- 30L wine making jugs are sold at Obi and Globus for about 20 Euros. Since you all know the other fine details needed, I am sure you can see that this still is conceivably made for under 70 Euros- {assuming you already own your power tools (Drill, appropriately sized drill bit, solderer) or have friends who own them. }

Using this pot still, making cuts, etc- I have produced about 5 litres thus far, and my first batch of "Speed Whiskey" was a huge success using frozen corn, barley, sugar and store bought bread yeast for a total cost of just under 3.50 Euros (all in) to produce about 1.2-1.5L of cut 65% good stuff.

With some innovation, brains, and hygienic sensibility for safe materials- {copper, stainless steel, glass, only}, you can produce a safe personal quantity easily in your kitchen (with the windows open) Using a basic electric hot plate again for about 20 Euros, I first heat the wash on my propane kitchen stove to about 140 F degrees, then transfer it to the electric for the higher temperatures, connect the worm with my clamp, apply the flour paste, (Electric has a very slow start up time- and fire heat from propane, allows a safe speed start after safely removed at 140 Degrees F.)

and 3 hours later, its a run.

Alas the clean up - :D

No problem- at a cost of 3.50 and electricity, I have top spirit in both quality and cost.

All critiques, praises, and observations are welcome.

Pictures to be included soon

Zwinzilious :D
kiwistiller
retired
Posts: 3215
Joined: Tue Mar 03, 2009 4:09 pm
Location: Auckland, NZ

Re: Micro Still 9 Litre Wonder

Post by kiwistiller »

Welcome along, sounds like you've been doing alright on your own though. :D
Three sheets to the wind!
My stuff
zwinzilious
Novice
Posts: 20
Joined: Tue Jul 20, 2010 3:26 am

Re: Micro Still 9 Litre Wonder

Post by zwinzilious »

Thanks!
zwinzilious
Novice
Posts: 20
Joined: Tue Jul 20, 2010 3:26 am

Re: Micro Still 9 Litre Wonder

Post by zwinzilious »

Picture of my second run
Cuts of newest second run of my first run
Cuts of newest second run of my first run
zwinzilious
Novice
Posts: 20
Joined: Tue Jul 20, 2010 3:26 am

Re: Micro Still 9 Litre Wonder

Post by zwinzilious »

I fill the tub with water, then put 2l frozen water bottles for cooling. The plastic around the ice prevents faster melting, while cooling the worm in combination with the water in the tub without the need for continuous water flow for 4-5 hours. 3 frozen 2L water bottles works perfect for one run.
Attachments
PICT4523.JPG
Kentucky shinner
Site Donor
Site Donor
Posts: 3017
Joined: Tue Jan 19, 2010 8:04 pm
Location: Paradise? Western KY

Re: Micro Still 9 Litre Wonder

Post by Kentucky shinner »

home engineering at its finest.
kingearwig
Bootlegger
Posts: 135
Joined: Sat Jan 19, 2008 12:51 am
Location: Indiana

Re: Micro Still 9 Litre Wonder

Post by kingearwig »

kiwistiller wrote:Welcome along, sounds like you've been doing alright on your own though. :D
Not quite on his own... :wink:
charles1001
Novice
Posts: 6
Joined: Sun Sep 12, 2010 3:04 pm

Re: Micro Still 9 Litre Wonder

Post by charles1001 »

love the design.
am looking into something simmilar myself as my pressure cooker still is deemed useless thanks to the rubber seal.
do you hold down the lid to the stock pot in any way or does it just sit on top happily without the need to be sealed, ie. is airtight?
thanks.
charles.
zwinzilious
Novice
Posts: 20
Joined: Tue Jul 20, 2010 3:26 am

Re: Micro Still 9 Litre Wonder

Post by zwinzilious »

Flour Paste and a tight belt through the handles works wonders. :D Zero vapor escape. The actual pressure of a run is minimal, even at higher temperatures
charles1001
Novice
Posts: 6
Joined: Sun Sep 12, 2010 3:04 pm

Re: Micro Still 9 Litre Wonder

Post by charles1001 »

brilliant! :D, didnt think of that! :lol: and the flower paste doesnt get into the wash?
loneswinger
Swill Maker
Posts: 413
Joined: Tue Sep 14, 2010 4:25 pm

Re: Micro Still 9 Litre Wonder

Post by loneswinger »

I like it too. Yep it is that easy. I still have 10 liter unit that I use for test batches. Just used it last night! Once your 'friends' find your hooch, that little guy might find it hard to keep up. (I say 'friends' in quotes because they didn't become that way until after I started stillin) If you can keep it out of there grubby hands, you should be just fine.

-Loneswinger
It's better to learn from other people's mistakes than your own.
zwinzilious
Novice
Posts: 20
Joined: Tue Jul 20, 2010 3:26 am

Re: Micro Still 9 Litre Wonder

Post by zwinzilious »

Credit is due to Kingearwig for the flour paste suggestion. (You won't be happy about that flour paste at clean up time though) 24 to 48 hours soaked in dishwasher soap, and some fierce scrubbing. Good as new- run number 2 :D
father william
Swill Maker
Posts: 194
Joined: Tue Mar 17, 2009 5:44 pm

Re: Micro Still 9 Litre Wonder

Post by father william »

I used to use a piece of pure natural latex surgical tubing, slit the long way, as a gasket between my 10 litre stock pot and the upside down stainless bowl on top of it. Still consider it a safe product (according to wiki latex dissolves in turpentine and naphtha but not ethanol/methanol etc), but I had persistent leakage problems where it overlapped. Also, the medical supply dealer where I bought it had an annoying habit of shorting me a couple of inches. Pretty pathetic on a three dollar purchase, but it kept happening.

Hit upon the alternative of an uncooked tortilla made of 1/4 cup white flour and 1/8 cup water, rolled out into a rectangular shape about 8" long and 2" wide. I roll the tortilla several times, folding it over onto itself like Damascus steel or a Samurai sword.

I cut it in half the long way, then cut each half in half again to get 4 8" strips. I wet both sides with a drip from the sink, then lay them down on the rim of the filled stock pot and push the edges over the inner and outer edge like an upside down "U". Overlap each joint about half an inch.

Haven't had a leak since I started doing it, and I no longer have to do business with unethical people. Don't know if it will work on your pot but it doesn't take all day to chip/clean off. I can get it off in about 5 minutes or less, both pot and bowl, using a wet Scotch Brite pad and a sponge. However, you'll find a few flour 'worms' in the pot when you dump it out. They get squeezed into the pot when pressure is applied to the joint.
If stupidity got us into this mess, then why can't it get us out?

Will Rogers
zwinzilious
Novice
Posts: 20
Joined: Tue Jul 20, 2010 3:26 am

Re: Micro Still 9 Litre Wonder

Post by zwinzilious »

Not sure about tortilla's, but flour is cheap, water is free, put the two together, and apply where you please ;)

As the pot gets hot, the flour paste bakes into a tight bonding vapor resistant seal, that for all intents and purposes- works every time. Just keep it on hand, and apply it where you see or hear vapor. In less that 2 minutes- sealed and problem solved.
rad14701
retired
Posts: 20865
Joined: Wed Dec 19, 2007 4:46 pm
Location: New York, USA

Re: Micro Still 9 Litre Wonder

Post by rad14701 »

zwinzilious wrote:Not sure about tortilla's, but flour is cheap, water is free, put the two together, and apply where you please ;)

As the pot gets hot, the flour paste bakes into a tight bonding vapor resistant seal, that for all intents and purposes- works every time. Just keep it on hand, and apply it where you see or hear vapor. In less that 2 minutes- sealed and problem solved.
The operative word here is "paste"... All too often I see folks attempting to use "dough"... I've never had a leak with flour paste... And if I need to reposition components before seals get rock hard I just re-wet the pasted joint and it re-seals without issue...
blanikdog
Angel's Share
Angel's Share
Posts: 4545
Joined: Tue Aug 09, 2005 11:55 pm
Location: Bullamakanka, Oztrailya

Re: Micro Still 9 Litre Wonder

Post by blanikdog »

Cannot beat flour paste. Why hobbiest's even bother with other shit fascinates me. :econfused:
Simple potstiller. Slow, single run.
(50 litre, propane heated pot still. Coil in bucket condenser - No thermometer, No carbon)
The Reading Lounge AND the Rules We Live By should be compulsory reading

Cumudgeon and loving it.
kiwistiller
retired
Posts: 3215
Joined: Tue Mar 03, 2009 4:09 pm
Location: Auckland, NZ

Re: Micro Still 9 Litre Wonder

Post by kiwistiller »

And you fascinate us, mate :lol:
Three sheets to the wind!
My stuff
gatorpizz
Novice
Posts: 13
Joined: Mon Jan 10, 2011 10:42 am
Location: BUCKEYE NATION

Re: Micro Still 9 Litre Wonder

Post by gatorpizz »

my new still is pretty close to this... I'll take some pictures and post for you entertainment
MAKING POPCORN PROUD 24/7
gatorpizz
Novice
Posts: 13
Joined: Mon Jan 10, 2011 10:42 am
Location: BUCKEYE NATION

Re: Micro Still 9 Litre Wonder

Post by gatorpizz »

Well, hey's my new still.. It'll hold 3 gallons without puking.

Image
still by bassplayinsweets, on Flickr
MAKING POPCORN PROUD 24/7
rad14701
retired
Posts: 20865
Joined: Wed Dec 19, 2007 4:46 pm
Location: New York, USA

Re: Micro Still 9 Litre Wonder

Post by rad14701 »

Nothing like a simple pot still to get started with, gatorpizz...
gatorpizz
Novice
Posts: 13
Joined: Mon Jan 10, 2011 10:42 am
Location: BUCKEYE NATION

Re: Micro Still 9 Litre Wonder

Post by gatorpizz »

rad14701 wrote:Nothing like a simple pot still to get started with, gatorpizz...

This is just something I whipped up for the apartment... dad has got a 25 gallon reflux back at the homestead :)
MAKING POPCORN PROUD 24/7
zwinzilious
Novice
Posts: 20
Joined: Tue Jul 20, 2010 3:26 am

Re: Micro Still 9 Litre Wonder

Post by zwinzilious »

I have had consistent success with this. Although I would like to take it up a notch and get something a bit bigger scale. Propane burner, beer keg, and start handy work on a column still, however the fact is, I am basically limited to a small balcony and kitchen with strict fire codes, preventing this + nosy neighbors.

These are the cards I am dealt.

The good news is, where you see the worm and a larger than usual cooling reservoir (ie my initial post pictures), I highly recommend one great innovation for others to try. Instead of just putting in ice for cooling the coil, I prefer to freeze solid several 1.5l or 2l plastic bottles then let them float above and have placed under the coil. Experience has shown that if the coil is cool, and the ABV is suitable in the wash, then the output is increased.

A typical run takes 6 hours, so at most I only use 5-6 frozen water filled plastic bottles. This provides maximum cooling, with minimum melting.

Also for my mash/wash vessels, I simply use two 5 liter glass bottles with locally available air locks. Everyone in this (EU country) traditionally ferments a number of products through the generations, and distills them also, so basic supplies are available at supermarkets. ie airlocks made of glass. Using a scaled down to proportion birdwatchers recipe, and the refrigerated baking yeast, has seen best results. It is debatable regarding champagne yeast. The end product is definitely refined, but for the cost to completion consideration, I am now sold on refrigerated bread yeast. It has the most powerful performance of all of them (yield, ABV etc) Miraculous and dirt cheap!

So Note for the Elders-

A first run yields 1.6 litres
Second run about .7litres

Typically I will save 3 first runs yield, combine the contents = 4.8 litres, so this combines 18 hours of runs
with 4 hours for this second run

2 run Likker yield = 2.1 Liters (approx) 70-75 %abv

I did one 3 distillation run, and got 85 %

Yes, a column puts my time and energy to shame, however, this is all done safely in my kitchen on an electric hot plate/burner.

It all adds up.
Attachments
PICT7102-1.JPG
Alpha and Omega
Alpha and Omega
zwinzilious
Novice
Posts: 20
Joined: Tue Jul 20, 2010 3:26 am

Re: Micro Still 9 Litre Wonder

Post by zwinzilious »

Just an update with a few pictures.

Part of the reason for that extra large reservoir of water I have the coil mounted in, was just pragmatic availability and suitability of materials where I live. Since I cannot constantly run water (this is in a kitchen, in a European country, with high taxes, water, util costs) it made sense to make use of greater volume of water to reduce the heating of the water. To help this process further, I was told to put ice in it. Then a thought occurred. Why not just freeze 1 and 2 liter bottles, and let them float freely in the reservoir and place them beneath the coil submerged in water. I tried this, and found they both cool efficiently, and melt very slowly. A good solution for others to try also.

My usual run takes 5-7 hours and in those 5 to seven hours, I used about 5 frozen bottles. The water stays at about 37 degrees at the base, and about 48 degrees (Fahrenheit) near the surface.

Another very useful tool is the (Ikea Stock pot, and especially the Ikea meat thermometer) modified for my use by drilling a hole through a wine cork and then having this reading provide guidance on the internal state of the pot still.

Following the basic guidance of temperatures on this site, I can distinguish the stages for "cutting" and knowing when the run is "Completed". 204-205 Fahrenheit.

Usual run yields about 1.2 liters.

I run 3 primary distillations, collect and store, and then run a second distillation, from the primaries.

At the moment this satisfies my requirements.

So my process goes like this

Birdwatchers Recipe converted to serve 10 litres put in two 5liter bottles, with a vapor lock. 3 weeks to complete typically
Next 3 runs of the 10 litres
Collection of about just under 4 litres
Add 3 litres water, then run the 2nd distilation.
Bottle, and dilute to 50%abv (flavor etc)

It does the job.

Recommendations and advice, gladly welcomed :thumbup:

Zwinzilious
Attachments
PICT7106.JPG
PICT7105.JPG
PICT7104.JPG
PICT7101.JPG
Titus-a-fishus
Swill Maker
Posts: 363
Joined: Sat May 22, 2010 3:03 pm
Location: Narnya....narnya business

Re: Micro Still 9 Litre Wonder

Post by Titus-a-fishus »

That last photo is a ripper.
You should take up photography as a side hobby

:ebiggrin: :D

Cheers
TAF
We haven't got the money so now we have to think
Build it, don't buy it
nil_fhios_agam
Novice
Posts: 32
Joined: Fri Jun 10, 2011 12:29 pm

Re: Micro Still 9 Litre Wonder

Post by nil_fhios_agam »

Hey - your still looks great. I am considering exactly the same for a test still.
Just a quick question, is the hole in the pot lid soldered or welded? Also, what type of fitting did you use? You say you're in a small apartment with strict fire safety regulations - just wondering how you managed to weld/solder the lid!? This is the only hurdle I have to jump to get my still up and running!
rad14701
retired
Posts: 20865
Joined: Wed Dec 19, 2007 4:46 pm
Location: New York, USA

Re: Micro Still 9 Litre Wonder

Post by rad14701 »

nil_fhios_agam wrote:Hey - your still looks great. I am considering exactly the same for a test still.
Just a quick question, is the hole in the pot lid soldered or welded? Also, what type of fitting did you use? You say you're in a small apartment with strict fire safety regulations - just wondering how you managed to weld/solder the lid!? This is the only hurdle I have to jump to get my still up and running!
Which member are you asking as there are three different designs being presented in this topic by two different members...???
nil_fhios_agam
Novice
Posts: 32
Joined: Fri Jun 10, 2011 12:29 pm

Re: Micro Still 9 Litre Wonder

Post by nil_fhios_agam »

rad14701 wrote:
nil_fhios_agam wrote:Hey - your still looks great. I am considering exactly the same for a test still.
Just a quick question, is the hole in the pot lid soldered or welded? Also, what type of fitting did you use? You say you're in a small apartment with strict fire safety regulations - just wondering how you managed to weld/solder the lid!? This is the only hurdle I have to jump to get my still up and running!
Which member are you asking as there are three different designs being presented in this topic by two different members...???
Ooopps, sorry. I was directing it at zwinzilious. However, if anyone wants to answer, that would be great too!
sparkmaster
Novice
Posts: 3
Joined: Thu Jun 16, 2011 8:22 pm

Re: Micro Still 9 Litre Wonder

Post by sparkmaster »

zwinzilious wrote:I fill the tub with water, then put 2l frozen water bottles for cooling. The plastic around the ice prevents faster melting, while cooling the worm in combination with the water in the tub without the need for continuous water flow for 4-5 hours. 3 frozen 2L water bottles works perfect for one run.

hi I am ignoring my wife as I peruse this site, a small suggestion as I do not know if you will think it silly. If you are going to add ice (and not salt it, as this may be very undoable) consider a small circulation pump to push the water about the tub. I make a lot of stock for soups and I use this method to cool 3 gallon batches faster so I can go to bed and not have it warm up my fridge. I noticed that if I didn't circulate the water it took longer. In the winter I take pots outside if possible and spin them in snow piles If I seat them and leave them they melt in, but much slower.

This is one of the neatest spots on the web!
rad14701
retired
Posts: 20865
Joined: Wed Dec 19, 2007 4:46 pm
Location: New York, USA

Re: Micro Still 9 Litre Wonder

Post by rad14701 »

sparkmaster wrote:
zwinzilious wrote:I fill the tub with water, then put 2l frozen water bottles for cooling. The plastic around the ice prevents faster melting, while cooling the worm in combination with the water in the tub without the need for continuous water flow for 4-5 hours. 3 frozen 2L water bottles works perfect for one run.

hi I am ignoring my wife as I peruse this site, a small suggestion as I do not know if you will think it silly. If you are going to add ice (and not salt it, as this may be very undoable) consider a small circulation pump to push the water about the tub. I make a lot of stock for soups and I use this method to cool 3 gallon batches faster so I can go to bed and not have it warm up my fridge. I noticed that if I didn't circulate the water it took longer. In the winter I take pots outside if possible and spin them in snow piles If I seat them and leave them they melt in, but much slower.

This is one of the neatest spots on the web!
Circulating the water in a flake stand (worm in a bucket) is not as effective as leaving the static water to rely on convection... Having the top get hot while the bottom remains cold maintains a temperature gradient throughout the worm rather than having the entire volume of cooling water gradually increase in temperature...
Post Reply