Clarification of wash before distilling - By Arroyo

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Single Malt Yinzer
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Clarification of wash before distilling - By Arroyo

Post by Single Malt Yinzer »

Stephen at Boston Apothecary nails a good article from Rafael Arroyo

Arroyo 1941: The “Tufo” (stink) of Crude Rum

https://www.bostonapothecary.com/arroyo ... crude-rum/" onclick="window.open(this.href);return false;" rel="nofollow
we had the opportunity to push our tests to the limit, acquiring the services of a yeast separating centrifuge, De Laval brand. We have been experimenting with this centrifuge for a few months, and we can say without fear of error that the results obtained so far fully meet all our requirements and even our demands. Below we will give the results obtained with this device in the separation of solids and elimination of “tufo” working with cane juice baticións:
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Re: Clarification of wash before distilling - By Arroyo

Post by Single Malt Yinzer »

Personally I've advocated keeping a lot of yeast in the wash for distilling. This may change my mind on it. I'll have to try some experiments
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Re: Clarification of wash before distilling - By Arroyo

Post by Saltbush Bill »

Very interesting SMY. Thank you for that link.
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Re: Clarification of wash before distilling - By Arroyo

Post by StillerBoy »

Thanks for the post SMY..

That explains why, in large part, why over the years in making sugar shine, I cleared the wash as well as could be done, by racking it a few times, and adding clarifier, I ended with some very nice neutral..

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Re: Clarification of wash before distilling - By Arroyo

Post by MtRainier »

Darnit. Now that I'm doing indirect heat and can have whatever I want in the wash without scorching there's a new reason to try to clarify it, heh.
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Re: Clarification of wash before distilling - By Arroyo

Post by StillerBoy »

MtRainier wrote:Now that I'm doing indirect heat and can have whatever I want in the wash without scorching
I wouldn't be to concern with clearing if you are using stream or a double boiler setup.. I'm of the view it more oriented towards direct heat..

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Re: Clarification of wash before distilling - By Arroyo

Post by shadylane »

Clearing definitely helps when trying to make a neutral with a wood fired potstill :wink: :lol:
On a side note. I love it when someone supplies a valuable link
Thank you SMY
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Re: Clarification of wash before distilling - By Arroyo

Post by OtisT »

Interesting read SMY. I think I need to read more of Arroyo’s stuff cauz everyone drops his name but I never know what the hell they are talking about.

Maybe I’m not on the same page, but I’ve never had issues with keeping the yeast out of my rum charge. Seems like by the time my rum ferment is done there is nothing but a thin layer of sediment and the rest looks pretty clear to me. (Dark, but clear). From a 35-40 gallon ferment I can rack off all but about a gallon with no sediment. Is that sediment what ya all are talking about, or is there a second clearing that I’m missing because I don’t let this sit long after racking?

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Re: Clarification of wash before distilling - By Arroyo

Post by shadylane »

MtRainier wrote:Darnit. Now that I'm doing indirect heat and can have whatever I want in the wash without scorching there's a new reason to try to clarify it, heh.
Don't look at it that way
Now you have a reason to build a centrifuge :lol:
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Re: Clarification of wash before distilling - By Arroyo

Post by Single Malt Yinzer »

They are literally removing all yeast cells that did not floculate. It's not simple clearing, it's complete removal. In "Whisky: Technology, Production and Marketing" they mention that Yamazaki and some other Japanese whiskey house both clarify purposefully to increase esters. Which up to now was always a conundrum as I thought that some yeast would be good for ester production.

https://www.youtube.com/watch?v=2F7KK76h14Y" onclick="window.open(this.href);return false;" rel="nofollow
https://www.youtube.com/watch?v=sDhueH3q6Y4" onclick="window.open(this.href);return false;" rel="nofollow

Even better: https://www.youtube.com/watch?v=dxTT_bP6IwI" onclick="window.open(this.href);return false;" rel="nofollow
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Re: Clarification of wash before distilling - By Arroyo

Post by Saltbush Bill »

I don't think people should jump to the conclusion that its going to be the end of the rum world if you don't clear the wash.
People have been making some very nice rums for several hundred years without clearing washes completely.
Some people may like the flavor that yeast in the wash leaves in the distillate.
Personally Ive always tried to let mine settle for a few weeks and left what rubbish I can in the fermenter.
It would be a boring world and an even more boring hobby if we all made booze that tasted the same using the same methods and liking the same flavors.
Arroyo printed a lot of good stuff about rum but that doesn't mean we all have to start using centrifuges to make decent Rum.
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Re: Clarification of wash before distilling - By Arroyo

Post by Yummyrum »

I agree Salty . And also lets not forget that we have the luxury of having time to settle washes . Commercial guys need to go straight from fermenter to still so a centrifuge is pretty much the only option .
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Re: Clarification of wash before distilling - By Arroyo

Post by NZChris »

The way I read it, Tufo is more an an issue for continuous distillation than for pot stills. A home distiller taking a foreshot off the stripping run already gets rid of quite a bit of the low boiling point nasties before it goes into the pot for the spirit run, so I won't be rushing out to buy a centrifuge yet.
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Re: Clarification of wash before distilling - By Arroyo

Post by Single Malt Yinzer »

Saltbush Bill wrote:that doesn't mean we all have to start using centrifuges to make decent Rum.
YES IT DOES! ARROYO SAID SO! I HAVE SIX ON ORDER RIGHT NOW! :twisted:

I agree. The reason I post these is so that we have more information to understand how different processes affect flavors of spirits. It's another tool for the distiller to use in guiding the development of their own spirit. If everyone used the same methods to make the same spirit I would consider it a failure. I love to see people post up "I am going to do X then Y then Z..." that makes me happy.
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Re: Clarification of wash before distilling - By Arroyo

Post by NZChris »

I know where there is a suitable centrifuge I could borrow and I could buy one tomorrow for about $300, so trying this is an option, but I'm not convinced by Arroyo's research that going to the trouble and expense of clarifying is going to make a significant difference to a non-commercial home pot distiller. If you were running a Jamaican style double thumper or a continuous column, I could see some value.

It may make a difference to those who run platers, but I don't so I'll leave it to them to comment on that.
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Re: Clarification of wash before distilling - By Arroyo

Post by Saltbush Bill »

I doubt its going to make a noticeable difference either even using plates.
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Re: Clarification of wash before distilling - By Arroyo

Post by Single Malt Yinzer »

He also advocated clarifying the molasses too. This gave him a very clean rum. To understand this he worked for Bicardi whose focus was creating a clean white rum that could be sold without aging. While we regard him for high ester rums processes, it was more of an off shoot of what not to do for a clean rum.
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Re: Clarification of wash before distilling - By Arroyo

Post by shadylane »

Single Malt Yinzer wrote:They are literally removing all yeast cells that did not floculate. It's not simple clearing, it's complete removal.
I'd like to see the equipment and process used. :wink:
Any ideas on how to remove +90% on the hobby scale :?:
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Re: Clarification of wash before distilling - By Arroyo

Post by NZChris »

shadylane wrote:Any ideas on how to remove +90% on the hobby scale :?:
Grandma's cream separator should work.
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Re: Clarification of wash before distilling - By Arroyo

Post by Yummyrum »

Oh lordy ... I’m picturing Butch’s washing machine again :esurprised:
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Re: Clarification of wash before distilling - By Arroyo

Post by Single Malt Yinzer »

shadylane wrote:I'd like to see the equipment and process used. :wink:
https://www.youtube.com/watch?v=XS666B7FV2g" onclick="window.open(this.href);return false;" rel="nofollow
shadylane wrote:Any ideas on how to remove +90% on the hobby scale :?:
http://www.centrifugefordummies.com/con ... -doing-oil" onclick="window.open(this.href);return false;" rel="nofollow

You can use a WVO (waste oil) centrifuge to achieve the same results. This would work for both clarifying molasses and the wash post fermentation. I think it's a bit much but if your thing is DYI then there's tons of tutorials out there.
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Re: Clarification of wash before distilling - By Arroyo

Post by 777 »

One possible method for yeast separation is crossflow membrane filtration with backflush. I have seen that used in commercial brewery as yeast removal process.
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Re: Clarification of wash before distilling - By Arroyo

Post by Syke »

1-micron filter pretty much removes all yeast. That's cheap and easy to procure and utilize.
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Re: Clarification of wash before distilling - By Arroyo

Post by 777 »

Syke wrote: Fri Sep 06, 2019 2:40 am 1-micron filter pretty much removes all yeast. That's cheap and easy to procure and utilize.
I did order parts for 1-micron water filter system with backflush option and I may test how it works for wash filtration
10" water filter cartridges are almost cheap and cartridge housing and L-type tree-way valves from china are neither expensive
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Re: Clarification of wash before distilling - By Arroyo

Post by LWTCS »

Notwithstanding the space needed for an additional fermenter, I think I'd rather have more fermentation capacity and just cold crash in a conical.

Commercial centrifuge has to cost as much (if not more) than a goodly sized fermenter is what I'm thinking?

Though it is probably true that you could probably free your fermentation tanks up faster with a centrifug?

There probably is a production threshold when a centrifuge makes sense for those that reckon a good brite rum beer is a requisite?
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Re: Clarification of wash before distilling - By Arroyo

Post by 777 »

Yes in commercial brewery waiting to yeast settle takes too much time but I don't really see using centrifuge for separating yeast as cost efficient method. High production rate centrifuge would be expensive I think it is perhaps more usable in hobby scale using batch method but too expensive. Cheaper method is filtration but maybe quality is a tad lower but should be good enough
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Re: Clarification of wash before distilling - By Arroyo

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Re: Clarification of wash before distilling - By Arroyo

Post by Corsaire »

As far as I understand Arroyo wanted to make flavorful rums. He even talks about competing with the Jamaicans. He further states that he feels batch distillation yields a better product than continuous.

He already had the centrifuge to pretreat his molasses, so for him the additional cost was lower.

And perhaps most importantly, he recommends a different yeast culture than what everybody uses, perhaps that yeast culture gives more undesirable flavors when it's not cleared from the wash?

I don't take everything he says as gospel truth. But I would like to experiment, as soon as I have a viable source of good molasses...
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Re: Clarification of wash before distilling - By Arroyo

Post by Jonnythesock »

Think making rum in winter is easier. When the mash is done I can wheel it outside over night for the yeast to crash: )
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Re: Clarification of wash before distilling - By Arroyo

Post by Saltbush Bill »

How is taking your wash for a walk easier than just leaving it sit in the corner to settle for a week or two ?
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