Vapor leak at union

Simple pot still distillation and construction with or without a thumper.

Moderator: Site Moderator

Post Reply
capt-n haddock
Novice
Posts: 19
Joined: Mon May 01, 2017 9:00 am

Vapor leak at union

Post by capt-n haddock »

Hi all,

I've made some upgrades to my pot still, so now it moves from a 2" riser from the keg, into a 2" 90* elbow and then stepping down into a 1' lateral, with a union, then into another 1" 90* elbow which then reduces down to 1/2" (with another union) for the liebig condenser (see photo).

where I seem to be leaking is @ the 1" union (the vapor does not seem to be coming from any of the sodded joints). So, what should I be trying to do to reduce the leak? or should I simply be using flour paste to stop up the leak?
union photo
union photo
If at first you don’t succeed, try, try again. Then quit. There’s no point in being a damn fool about it.
User avatar
acfixer69
Global moderator
Posts: 4847
Joined: Mon Dec 20, 2010 3:34 pm
Location: CT USA

Re: Vapor leak at union

Post by acfixer69 »

Since it's a mechanical joint connection break it open and look at the faces. It is not unusual for solder to run there if you are not doing soldering as a payday. Also unions halves are not interchangeable from different manufacturers.
StillerBoy
Master of Distillation
Posts: 3387
Joined: Thu Dec 01, 2016 6:27 pm
Location: Ontario

Re: Vapor leak at union

Post by StillerBoy »

As acfixer stated about solder that may have run onto the mating surface.. and you may need to lightly work over the mating surfaces with some fine sandpaper to remove some debris left during the manufacturing process.. also clean the threads with some scotch brite pad, because sometime the threads are poorly made and leave a rough surface which makes it hard to tighten good enough..

Mars
" I know quite certainly that I myself have no special talent. Curiosity, Obsession and dogged endurance, combined with self-criticism, have brought me to my knowledge and understanding "

– Albert Einstein
capt-n haddock
Novice
Posts: 19
Joined: Mon May 01, 2017 9:00 am

Re: Vapor leak at union

Post by capt-n haddock »

alright, I'll give those points a try. thanks!
If at first you don’t succeed, try, try again. Then quit. There’s no point in being a damn fool about it.
User avatar
still_stirrin
Master of Distillation
Posts: 10344
Joined: Tue Mar 18, 2014 7:01 am
Location: where the buffalo roam, and the deer & antelope play

Re: Vapor leak at union

Post by still_stirrin »

Use PTFE (plumber's) tape on the union threads. It'll allow you to draw in the union tighter.

Also, I usually allow a little to wrap in the cup socket too when I wrap the threads. When the halves come together, the tape will help it close tighter (easier) without galling (copper has a tendency to gall with itself).
ss
My LM/VM & Potstill: My build thread
My Cadco hotplate modification thread: Hotplate Build
My stock pot gin still: stock pot potstill
My 5-grain Bourbon recipe: Special K
User avatar
NZChris
Master of Distillation
Posts: 13125
Joined: Tue Apr 23, 2013 2:42 am
Location: New Zealand

Re: Vapor leak at union

Post by NZChris »

Vapor leaks are often caused by a blockage, and blockages are dangerous, so check for that first.
capt-n haddock
Novice
Posts: 19
Joined: Mon May 01, 2017 9:00 am

Re: Vapor leak at union

Post by capt-n haddock »

no, no blockages. but thanks for your concern. I can and have visually verified all of my piping. I guess I should mention that I noticed this during my vinegar & trash wash runs.
If at first you don’t succeed, try, try again. Then quit. There’s no point in being a damn fool about it.
capt-n haddock
Novice
Posts: 19
Joined: Mon May 01, 2017 9:00 am

Re: Vapor leak at union

Post by capt-n haddock »

regarding the face of the union, if that's the issue, is there a good way to make the two surfaces mate better (or is this simply a matter of sanding down any rough edges)?
If at first you don’t succeed, try, try again. Then quit. There’s no point in being a damn fool about it.
User avatar
acfixer69
Global moderator
Posts: 4847
Joined: Mon Dec 20, 2010 3:34 pm
Location: CT USA

Re: Vapor leak at union

Post by acfixer69 »

capt-n haddock wrote:regarding the face of the union, if that's the issue, is there a good way to make the two surfaces mate better (or is this simply a matter of sanding down any rough edges)?
If it's a flaw in the union faces you may be able to use some lapin compound or jewelers rouge to seat it but if it is not a mating pair I would toss it and go with a new one. I would use ferrules to relapse it but that's me.
OtisT
Master of Distillation
Posts: 3189
Joined: Sat Oct 24, 2015 11:59 am
Location: Pacific Northwest

Re: Vapor leak at union

Post by OtisT »

You need to make sure that the copper nipple and cup (for lack of better terms) are aligned perfectly before threading the brass nut to the copper threads. I find tightening threads does not bring a misaligned Union into alignment. Otis
Otis’ Pot and Thumper, Dimroth Condenser: Pot-n-Thumper/Dimroth
Learning to Toast: Toasting Wood
Polishing Spirits with Fruitwood: Fruitwood
Badmotivator’s Barrels: Badmo Barrels
User avatar
Swedish Pride
Site Donor
Site Donor
Posts: 2660
Joined: Tue Aug 26, 2014 2:16 am
Location: Emerald Isle

Re: Vapor leak at union

Post by Swedish Pride »

still_stirrin wrote:Use PTFE (plumber's) tape on the union threads. It'll allow you to draw in the union tighter.....
+1

bet it'll sort the problem at hand
Don't be a dick
User avatar
BlackStrap
Swill Maker
Posts: 301
Joined: Thu Mar 02, 2017 3:48 pm
Location: The hills of Appalachia

Re: Vapor leak at union

Post by BlackStrap »

I use copper unions in my steam stripper setup, connecting the 2 boilers together. When I was fitting everything up and soldering things together the connections between the 2 boilers is interchangeable physically.
Unions.jpg
However when flipped end for end the one union connection has a slow drip (It's water vapor, so no worries BUT it bugs the %^& out of me)...

In other words the union halves are not interchangeable or a slight mismatch causing my drip...

My Solution.
Mark the direction of vapor, ( Sharpy marker works)
Take apart the unions,
Check the mating surfaces, There will be some discoloration where the mate together.
Polish if need be, and always assemble in the same direction.

+1 Like others have said PTFE tape works well and keeps things dry and from gulling up.
Most questions can be answered here http://homedistiller.org/ and here http://homedistiller.org/forum/viewforum.php?f=46

The one who cuts the firewood gets twice the warmth
User avatar
bronctoad
Site Donor
Site Donor
Posts: 165
Joined: Sat Oct 15, 2016 5:16 pm
Location: middle of vacationland

Re: Vapor leak at union

Post by bronctoad »

On my old rig I had the same set up as your picture, mine also leaked at that joint.
what I found to worked well is 3 or 4 wraps of ptfe tape on the ball of the union.
when applying the tape keep it stretched tight so the tape on the pipe side of the ball
wont interfere with the nut coming up against the ball. you might have to work the nut
opposite of the tape wraps a couple of turns to get it over the ptfe with out balling it up.
that trick will worked but you have to make sure your union is in position before you tighten
it up. you cant rotate the union faces after its been snugged, so assemble your whole rig
then tighten all the fittings. you also have to replace it every time, tedious but it works.

Bronctoad
User avatar
Chauncey
Site Donor
Site Donor
Posts: 1570
Joined: Sat Feb 06, 2016 1:30 am
Location: NOLA

Re: Vapor leak at union

Post by Chauncey »

still_stirrin wrote:Use PTFE (plumber's) tape on the union threads. It'll allow you to draw in the union tighter.

Also, I usually allow a little to wrap in the cup socket too when I wrap the threads. When the halves come together, the tape will help it close tighter (easier) without galling (copper has a tendency to gall with itself).
ss
This

I find Union leaks are fixed by PTFE taping the socket side only. Even though a wrap on the threads def isn't gonna hurt. I had read it somewhere in the forum tried it once now I tapem every time and haven't had a leak since
<no stopping to corner anytime [] no parking passenger zone>

When people tell me I'll regret that in the morning, I sleep till noon.
capt-n haddock
Novice
Posts: 19
Joined: Mon May 01, 2017 9:00 am

Re: Vapor leak at union

Post by capt-n haddock »

Allmyexsliveinhell : Geaux Saints!

Then, thanks for all the responses everyone. In pulling apart the union, it seems like the ball & socket simply won't be a tight fit (they were bought as a unit, but I never paid any attention to the quality of the fitting until now), baring me doing a lot of filing on the socket to make it work. which seems like a fools errand really. So what I see is that I have two choices: find a new quality union with good fitment, or find a 1" tri-clamp ferrule.

My plan has been to upgrade to tri-clamps all along, but when I look for 1" clamps, i'm not seeing anything other than SS ferrules (seems like 1.5" is the smallest copper ferrule that I can find. And while I like SS, I have no idea how hard it would be to solder to copper. Any guidance there?
If at first you don’t succeed, try, try again. Then quit. There’s no point in being a damn fool about it.
cob
Master of Distillation
Posts: 2691
Joined: Sun Jul 26, 2009 4:38 pm
Location: little puffs of dust where my feet used to be

Re: Vapor leak at union

Post by cob »

acfixer69 wrote:
capt-n haddock wrote:regarding the face of the union, if that's the issue, is there a good way to make the two surfaces mate better (or is this simply a matter of sanding down any rough edges)?
If it's a flaw in the union faces you may be able to use some lapin compound or jewelers rouge to seat it but if it is not a mating pair I would toss it and go with a new one. I would use ferrules to relapse it but that's me.
this is the least expensive and most practical advice given. it will work.

you can use almost any toothpaste as lapping compound.

just put the joint together loosely with compound and rotate until you have a polish line around both pieces.
be water my friend
User avatar
Kareltje
Distiller
Posts: 2176
Joined: Tue Feb 09, 2016 4:29 pm

Re: Vapor leak at union

Post by Kareltje »

Sometimes I find some of the unions sweat a bit. Drop by drop and when I collect these drops, they do not contain any alcohol. So I don not care much about it, just put some white tape around them if need be.
But of course your leaks might be different.
capt-n haddock
Novice
Posts: 19
Joined: Mon May 01, 2017 9:00 am

Re: Vapor leak at union

Post by capt-n haddock »

Kareltje wrote:Sometimes I find some of the unions sweat a bit. Drop by drop and when I collect these drops, they do not contain any alcohol. So I don not care much about it, just put some white tape around them if need be.
But of course your leaks might be different.
in this case, because I was doing the vinegar run, I was able to taste the condensate leaking out of the union, and it was vinegar, same with the vapor coming from the union. what's interesting is that I pulled the still apart today, and was looking at the union, and you could see the staining of the vinegar on the ball & socket where the joint is not mating fully.

it seems like the shoulder of the socket is not deep enough / wide enough to mate fully with the ball.
If at first you don’t succeed, try, try again. Then quit. There’s no point in being a damn fool about it.
User avatar
still_stirrin
Master of Distillation
Posts: 10344
Joined: Tue Mar 18, 2014 7:01 am
Location: where the buffalo roam, and the deer & antelope play

Re: Vapor leak at union

Post by still_stirrin »

You can use some fine sandpaper/emory cloth to reduce the “shoulder” a little. But, PTFE will help you in the end. (experience with this).
ss
My LM/VM & Potstill: My build thread
My Cadco hotplate modification thread: Hotplate Build
My stock pot gin still: stock pot potstill
My 5-grain Bourbon recipe: Special K
User avatar
Chauncey
Site Donor
Site Donor
Posts: 1570
Joined: Sat Feb 06, 2016 1:30 am
Location: NOLA

Re: Vapor leak at union

Post by Chauncey »

cob wrote:
acfixer69 wrote:
capt-n haddock wrote:regarding the face of the union, if that's the issue, is there a good way to make the two surfaces mate better (or is this simply a matter of sanding down any rough edges)?
If it's a flaw in the union faces you may be able to use some lapin compound or jewelers rouge to seat it but if it is not a mating pair I would toss it and go with a new one. I would use ferrules to relapse it but that's me.
this is the least expensive and most practical advice given. it will work.

you can use almost any toothpaste as lapping compound.

just put the joint together loosely with compound and rotate until you have a polish line around both pieces.
is there a brand of toothpaste that is prefered for this? just curious for my future reference. i figure toms of maine or perodontax or colgate or crest might be of very different grittinessess(sic) and work differently.


also to the OP regarding finding smaller tri clamp ferrules you could just flare/flange it out yourself. ive seen smaller diameter tubing flared for TCs before.
<no stopping to corner anytime [] no parking passenger zone>

When people tell me I'll regret that in the morning, I sleep till noon.
cob
Master of Distillation
Posts: 2691
Joined: Sun Jul 26, 2009 4:38 pm
Location: little puffs of dust where my feet used to be

Re: Vapor leak at union

Post by cob »

Allmyexsliveinhell wrote:
cob wrote:
acfixer69 wrote:
capt-n haddock wrote:regarding the face of the union, if that's the issue, is there a good way to make the two surfaces mate better (or is this simply a matter of sanding down any rough edges)?
If it's a flaw in the union faces you may be able to use some lapin compound or jewelers rouge to seat it but if it is not a mating pair I would toss it and go with a new one. I would use ferrules to relapse it but that's me.
this is the least expensive and most practical advice given. it will work.

you can use almost any toothpaste as lapping compound.

just put the joint together loosely with compound and rotate until you have a polish line around both pieces.
is there a brand of toothpaste that is prefered for this? just curious for my future reference. i figure toms of maine or perodontax or colgate or crest might be of very different grittinessess(sic) and work differently.


also to the OP regarding finding smaller tri clamp ferrules you could just flare/flange it out yourself. ive seen smaller diameter tubing flared for TCs before.
brand doesn't matter most toothpastes have either silica or calcium carbonate as abrasive ingredients,

and cleanup is easier than a grease based lapping compound. the grit is close to the same for most toothpaste.
be water my friend
User avatar
Chauncey
Site Donor
Site Donor
Posts: 1570
Joined: Sat Feb 06, 2016 1:30 am
Location: NOLA

Re: Vapor leak at union

Post by Chauncey »

Cool. Good to know.
<no stopping to corner anytime [] no parking passenger zone>

When people tell me I'll regret that in the morning, I sleep till noon.
Post Reply