VM Liebig condenser to valve to column connection

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Big L
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VM Liebig condenser to valve to column connection

Post by Big L »

Hi All,

This part just arrived, I must have not understood the picture properly as its not quite as i expected it to be..

https://www.aliexpress.com/item/3288526 ... 4c4dHw2tsB


The section that attaches to the column has a lip and i am a bit worried this will impact vapor product flow. As indicated in my diagram below will the flow path of V still be possible? I am concerned this part is in fact for a LM still rather than the VM i am trying to build. (not included in the drawing is a coil condenser above for reflux)
still1.jpg
Also on a side note (minus some missing tube and a slightly bent condenser coil) all the stuff arrived promptish (36 days) from China

Thanks Everyone
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Bushman
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Re: VM Liebig condenser to valve to column connection

Post by Bushman »

Your diagram does not match the link? Do you have to build your own column? Looks as if the product part of the still is too close to where it will attach to the column in order for it to clear the boiler. Not sure if this makes sense to you but the link still from china just looks a bit tight.
StillerBoy
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Re: VM Liebig condenser to valve to column connection

Post by StillerBoy »

What you have purchase cup with a valve and a mini liebig.. its called a vapor throat body.. as the vapors are condensed by a condenser about the cup, the liquid flows down into the cup, and can be extracted by open the valve, or allow to over flow and be refluxed in the column below it..

That item would work well on a concentric design..

Mars
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Big L
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Re: VM Liebig condenser to valve to column connection

Post by Big L »

Ah yes that makes sense. daym okay i'll just make this section out of copper then :)
OtisT
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Re: VM Liebig condenser to valve to column connection

Post by OtisT »

Your concern is well founded. That’s not gonna work at all as a VM head.

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StillerBoy
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Re: VM Liebig condenser to valve to column connection

Post by StillerBoy »

StillerBoy wrote: Tue May 26, 2020 6:50 am That item would work well on a concentric design..
Here's a couple of pictures showing a vapor throat body on a concentric is built and works..

Mars
DSC014511.jpg
DSC014561.jpg
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Twisted Brick
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Re: VM Liebig condenser to valve to column connection

Post by Twisted Brick »

StillerBoy wrote: Tue May 26, 2020 6:50 am What you have purchase cup with a valve and a mini liebig.. its called a vapor throat body.. as the vapors are condensed by a condenser about the cup, the liquid flows down into the cup, and can be extracted by open the valve, or allow to over flow and be refluxed in the column below it..

That item would work well on a concentric design..

Mars
I thought that looked just like Rad's still!
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Yummyrum
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Re: VM Liebig condenser to valve to column connection

Post by Yummyrum »

I’m thinking if you flipped it upside down , it would then be a VM :wink:
Can’ say how well it would work , but worth a try .
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Danespirit
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Re: VM Liebig condenser to valve to column connection

Post by Danespirit »

The part you linked to is an LM still head, yes.
To improve the product takeoff a "roof" over the inner pipe is helpful.
Vapor can still pass but everything condensed by the RC is lead to the void in between the two pipes...the rest overflows into the column again.
You can use this LM section (with or without the improvement I mentioned) and build a VM on top of that.
That will give you the option for an LM/VM combo a lot of members here are running with great success.
Btw..a conversion to a CCVM/LM combo is still possible by letting the VM section being on top of the LM.
By doing so you eliminate the costly valve needed for a traditional VM setup. :idea:

Edit: The flow path you've drawn won't happen.
It's against the laws of thermodynamics.
It will still be in the vapor phase as it passes the restriction/inner tube and moves up to the RC on top.
From there it condenses and falls as reflux downwards...(there the improvement with the "roof" comes in).
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Re: VM Liebig condenser to valve to column connection

Post by bluefish_dist »

A easier to build version of what you drew is the two cups boka design. Just place a cut off T as a roof in the upper condenser section and then you don’t have to do a concentric condenser.

To make it a lm/vm, then add another T in the small diameter pipe and add a valve. Now it’s a vm as well. Makes the valve cheaper as it’s smaller.
Last edited by bluefish_dist on Thu May 28, 2020 6:37 am, edited 1 time in total.
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Big L
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Re: VM Liebig condenser to valve to column connection

Post by Big L »

bluefish_dist wrote: Wed May 27, 2020 10:05 am A easier to build version of what you drew is the two cups boka design. Just place a cut off T as a roof in the upper condenser section and then you don’t have to do a concentric condenser.

To make it a lm/vm, then add another 90 in the small diameter pipe and add a valve. Now it’s a vm as well. Makes the valve cheaper as it’s smaller.
Do you mean this basically?
90bend.jpg
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Re: VM Liebig condenser to valve to column connection

Post by bluefish_dist »

F7224D27-2266-443F-98CD-942AA8288E51.jpeg
F7224D27-2266-443F-98CD-942AA8288E51.jpeg
Like this.
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Danespirit
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Re: VM Liebig condenser to valve to column connection

Post by Danespirit »

+1 Bluefish.

Something like this is what I had in mind with an LM/VM combo.
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bluefish_dist
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Re: VM Liebig condenser to valve to column connection

Post by bluefish_dist »

That was how I built my first still head. I also added an external return line so the falling distillate was introduced below the takeoff and above the packing. Worked well. I eventually changed to my current design as it required a minimal amount of welding and was shorter.
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Yummyrum
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Re: VM Liebig condenser to valve to column connection

Post by Yummyrum »

The dual reducer is a good design . I also used it on my 2” LM/VM still head .
OK , it’s a bit weirded out , but I was hoping to keep all my options open so it was designed so I could do reverse LM down the track .: Turns out , VM was streaks ahead straight off the bat .
9B3A338B-412C-4660-B498-695889A7756D.jpeg
9B3A338B-412C-4660-B498-695889A7756D.jpeg (21.27 KiB) Viewed 1574 times
viewtopic.php?f=17&t=67194#p7481508
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bluefish_dist
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Re: VM Liebig condenser to valve to column connection

Post by bluefish_dist »

Yummy, always wanted to try a reverse lm. Glad to hear I am not missing anything. That looks almost like my first still head except the lm valve was off the external pipe with a T.
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