"Sour" still

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rug
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"Sour" still

Post by rug »

Hi.
My still, or more precise my boiling kettle and CM has gone sour.
Smells like if I have vommited into it. The destilled product get a "sour smell" ....
Why?
What to do?
:sick:
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still_stirrin
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Re: "Sour" still

Post by still_stirrin »

More info needed:

1) what material is the boiler?
2) what material is the CM reflux head?
3) when was the still last used?
4) what type of wash did you run?
5) have done a cleaning run?
6) did you use any special post-run protocol?
7) how do you store your still?

Perhaps something crawled in and died.
ss
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Corn Cracker
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Re: "Sour" still

Post by Corn Cracker »

Sounds like you did not get it as clean as you thought after your last run
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Demy
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Re: "Sour" still

Post by Demy »

As Stillstirrin said you need to give more information to give you an answer.
MihiT
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Re: "Sour" still

Post by MihiT »

.
Demy wrote: Thu Nov 04, 2021 3:24 am As Stillstirrin said you need to give more information to give you an answer.
Not really...
rug wrote: Wed Nov 03, 2021 11:29 pm What to do?
:sick:
Clean it. Vinegar run. Sac run.
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Stonecutter
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Re: "Sour" still

Post by Stonecutter »

Like SS said, in order to give good info we need good info. Do you use any cleaning agents?
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kimbodious
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Re: "Sour" still

Post by kimbodious »

Tails in the packing will do this.The other issue could be a copper plated steel pot scrubber that has badly corroded. No need to ask how I know these things.
--
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rug
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Re: "Sour" still

Post by rug »

still_stirrin wrote: Thu Nov 04, 2021 2:44 am More info needed:

1) what material is the boiler?
Steinless steel
2) what material is the CM reflux head?
Stainless steel cm filled with copper scrubs.
3) when was the still last used?
Recently
4) what type of wash did you run?
Sugar, yeast, gin-spices
5) have done a cleaning run?
No, an old still used for years
6) did you use any special post-run protocol?
No, should I?
7) how do you store your still?
Dry, dark and cold :)
8) Perhaps something crawled in and died.
Hehe, well, I just found a dead mouse in my car so maybe one in the CM? :D

ss
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dragon9874
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Re: "Sour" still

Post by dragon9874 »

MihiT wrote: Thu Nov 04, 2021 2:52 pm
rug wrote: Wed Nov 03, 2021 11:29 pm What to do?
:sick:
Clean it. Vinegar run. Sac run.
bingo... bango... bongo. always start there!! d-(^_^)-b

it's like a reboot of a computer/system. when in doubt, reboot. translates here to... wait for it........

"When in doubt, clean it out!" vinegar/water (50/50) HOT & HARD for an hour (+/-, some will say 30 mins), then your sacrificial run (SW/BW). then, try another run, go from there. good luck!!

edit: added the water part to the vinegar, don't want anyone using 100%. ;-)
My Journey Started here: Cranky's Spoon Feeding!
10G pot still + 3.5G thumper + 4G condenser... all copper! d-(^^,)
{DWDSD} \m/(^_^) \m/
cob
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Re: "Sour" still

Post by cob »

this is one of several posts on HD that state for a vinegar cleaning run use

50% vinegar and 50% water. this is misleading as store bought vinegar is

already 5% vinegar and 95% water. so the correct ratio for a cleaning run

is 2.5% vinegar and 97.5% water. 100% vinegar is quite acidic and likely

difficult to obtain. stronger solutions than 5% are available for non home

uses but not readily available outside of industrial suppliers. so

50% store bought vinegar (5%) and 50% water is the correct cleaning ratio.

I would hate for someone with access to 75% vinegar to use it at that strength.
be water my friend
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dragon9874
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Re: "Sour" still

Post by dragon9874 »

cob wrote: Tue Dec 14, 2021 4:55 pm ...50% store bought vinegar (5%) and 50% water is the correct cleaning ratio.
thx Cob!! d-(^^,)

during the 1st part of your reply, i was like: "man, i've been doing it "WRONG" this whole time?!?" but you talked me off the ledge w/ the latter part of y your post. 50/50 is the mark (for your 'typical', grocery store purchased white vinegar). you would potentially need to FURTHER dilute (by possibly quite a bit) if using a more powerful vinegar, such as POSSIBLY some (or all of) the afore mentioned ones. thx for the schooling Cob!

LOVE IT!!! :-)
~web
My Journey Started here: Cranky's Spoon Feeding!
10G pot still + 3.5G thumper + 4G condenser... all copper! d-(^^,)
{DWDSD} \m/(^_^) \m/
MihiT
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Re: "Sour" still

Post by MihiT »

cob wrote: Tue Dec 14, 2021 4:55 pm this is one of several posts on HD that state for a vinegar cleaning run use

50% vinegar and 50% water. this is misleading as store bought vinegar is

already 5% vinegar and 95% water. so the correct ratio for a cleaning run
Well... yeah nah.
Acetic acid is a constituent component of vinegar. I think to be called or sold as vinegar it needs to be 4-8% acetic acid. (The balance being water and insolubles)(and if you make your own vinegar with wild aerobics you'll generally end up at a similar acid concentration)

If one was buying pure, or lab grade acids, then yes. But anything you can buy as "vinegar"... 50-50 is about correct.
ThomasBrewer
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Re: "Sour" still

Post by ThomasBrewer »

Exactly, MihiT. No one is confusing glacial acetic acid or acetic anhydride with vinegar.
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