"Sour" still
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"Sour" still
Hi.
My still, or more precise my boiling kettle and CM has gone sour.
Smells like if I have vommited into it. The destilled product get a "sour smell" ....
Why?
What to do?
My still, or more precise my boiling kettle and CM has gone sour.
Smells like if I have vommited into it. The destilled product get a "sour smell" ....
Why?
What to do?
- still_stirrin
- Master of Distillation
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Re: "Sour" still
More info needed:
1) what material is the boiler?
2) what material is the CM reflux head?
3) when was the still last used?
4) what type of wash did you run?
5) have done a cleaning run?
6) did you use any special post-run protocol?
7) how do you store your still?
Perhaps something crawled in and died.
ss
1) what material is the boiler?
2) what material is the CM reflux head?
3) when was the still last used?
4) what type of wash did you run?
5) have done a cleaning run?
6) did you use any special post-run protocol?
7) how do you store your still?
Perhaps something crawled in and died.
ss
My LM/VM & Potstill: My build thread
My Cadco hotplate modification thread: Hotplate Build
My stock pot gin still: stock pot potstill
My 5-grain Bourbon recipe: Special K
My Cadco hotplate modification thread: Hotplate Build
My stock pot gin still: stock pot potstill
My 5-grain Bourbon recipe: Special K
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- Swill Maker
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Re: "Sour" still
Sounds like you did not get it as clean as you thought after your last run
"To ease the pressures of this world here's the way i got it figured, the thing to do for me and you is to drink lots of good corn liquor"
Buck Owens
Buck Owens
Re: "Sour" still
As Stillstirrin said you need to give more information to give you an answer.
- Stonecutter
- Distiller
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Re: "Sour" still
Like SS said, in order to give good info we need good info. Do you use any cleaning agents?
Freedom had been hunted round the globe; reason was considered as rebellion; and the slavery of fear had made men afraid to think. But such is the irresistible nature of truth, that all it asks, and all it wants, is the liberty of appearing.
-Thomas Paine
-Thomas Paine
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- Distiller
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Re: "Sour" still
Tails in the packing will do this.The other issue could be a copper plated steel pot scrubber that has badly corroded. No need to ask how I know these things.
--
50L Beer keg boiler, 2200W element
Modular 2" Pot Still
opinions are free and everybody has them, experience costs you time
50L Beer keg boiler, 2200W element
Modular 2" Pot Still
opinions are free and everybody has them, experience costs you time
Re: "Sour" still
still_stirrin wrote: ↑Thu Nov 04, 2021 2:44 am More info needed:
1) what material is the boiler?
Steinless steel
2) what material is the CM reflux head?
Stainless steel cm filled with copper scrubs.
3) when was the still last used?
Recently
4) what type of wash did you run?
Sugar, yeast, gin-spices
5) have done a cleaning run?
No, an old still used for years
6) did you use any special post-run protocol?
No, should I?
7) how do you store your still?
Dry, dark and cold
Perhaps something crawled in and died.
Hehe, well, I just found a dead mouse in my car so maybe one in the CM?
ss
- dragon9874
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Re: "Sour" still
bingo... bango... bongo. always start there!! d-(^_^)-b
it's like a reboot of a computer/system. when in doubt, reboot. translates here to... wait for it........
"When in doubt, clean it out!" vinegar/water (50/50) HOT & HARD for an hour (+/-, some will say 30 mins), then your sacrificial run (SW/BW). then, try another run, go from there. good luck!!
edit: added the water part to the vinegar, don't want anyone using 100%.
My Journey Started here: Cranky's Spoon Feeding!
10G pot still + 3.5G thumper + 4G condenser... all copper! d-(^^,)
{DWDSD} \m/(^_^) \m/
10G pot still + 3.5G thumper + 4G condenser... all copper! d-(^^,)
{DWDSD} \m/(^_^) \m/
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- Master of Distillation
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Re: "Sour" still
this is one of several posts on HD that state for a vinegar cleaning run use
50% vinegar and 50% water. this is misleading as store bought vinegar is
already 5% vinegar and 95% water. so the correct ratio for a cleaning run
is 2.5% vinegar and 97.5% water. 100% vinegar is quite acidic and likely
difficult to obtain. stronger solutions than 5% are available for non home
uses but not readily available outside of industrial suppliers. so
50% store bought vinegar (5%) and 50% water is the correct cleaning ratio.
I would hate for someone with access to 75% vinegar to use it at that strength.
50% vinegar and 50% water. this is misleading as store bought vinegar is
already 5% vinegar and 95% water. so the correct ratio for a cleaning run
is 2.5% vinegar and 97.5% water. 100% vinegar is quite acidic and likely
difficult to obtain. stronger solutions than 5% are available for non home
uses but not readily available outside of industrial suppliers. so
50% store bought vinegar (5%) and 50% water is the correct cleaning ratio.
I would hate for someone with access to 75% vinegar to use it at that strength.
be water my friend
- dragon9874
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Re: "Sour" still
thx Cob!! d-(^^,)
during the 1st part of your reply, i was like: "man, i've been doing it "WRONG" this whole time?!?" but you talked me off the ledge w/ the latter part of y your post. 50/50 is the mark (for your 'typical', grocery store purchased white vinegar). you would potentially need to FURTHER dilute (by possibly quite a bit) if using a more powerful vinegar, such as POSSIBLY some (or all of) the afore mentioned ones. thx for the schooling Cob!
LOVE IT!!!
~web
My Journey Started here: Cranky's Spoon Feeding!
10G pot still + 3.5G thumper + 4G condenser... all copper! d-(^^,)
{DWDSD} \m/(^_^) \m/
10G pot still + 3.5G thumper + 4G condenser... all copper! d-(^^,)
{DWDSD} \m/(^_^) \m/
Re: "Sour" still
Well... yeah nah.
Acetic acid is a constituent component of vinegar. I think to be called or sold as vinegar it needs to be 4-8% acetic acid. (The balance being water and insolubles)(and if you make your own vinegar with wild aerobics you'll generally end up at a similar acid concentration)
If one was buying pure, or lab grade acids, then yes. But anything you can buy as "vinegar"... 50-50 is about correct.
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- Swill Maker
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Re: "Sour" still
Exactly, MihiT. No one is confusing glacial acetic acid or acetic anhydride with vinegar.