Recent Locked Thread
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Recent Locked Thread
Hey gang,
Didn't want to get to the point where folks get undignified or anything. There was definitely some confusion and lack of context (or maybe irrelevant context?) on that thread beyond the PID debate.
Was just looking to politely comment about a couple of talking points used. My comments surely would have pulled the thread into another direction all together.
A really (really, really ) old timer once asked me to only talk about what I know. Hopefully I can articulate?
The first thing to really stick out toward the end of that thread was this:
All fuel and alcohol distillation takes place by temperature. Methanol for example is one of the first things to come off at low temps, followed by other foreshots components, then comes your heads at slightly higher temperatures. Then hearts come off next at higher temperatures, followed by tails. The key being each of these come off at progressively higher temperatures.
Please have a read through this write up to gain a bit more clarity about Methanol:
This next comment is absolutely lacking anything substantive:
Big industrial continuous stills have multiple take-off points at different plate levels to take spirits at temperature. Each plate will have a different temperature. Same concept just handled differently.
Operationally, you can't compare temps on a batch system to temps on a continuous system. Batch system temps are ever changing. Batch temps have to change. No choice.
Continuous systems are tuned to run in steady state. This steady state tuning is entirely predicated upon the fact that an alcoholic(beer) mixture is continuously being fed into the system. At no point is any part of the system EVER depleted of alcohol as long as the system is being fed.
Steady state systems do very well with PIDs controlling various operations. But the one thing PIDs do not control as HDNB mentions is heat input to the system. PIDs (or the like) control pump speeds and coolant flow speeds.
As far as pulling product according to fractions are concerned again this concept is predicated upon a continuous feed of a reliably consistent alcoholic beer mixture. As an aside, product is taken off in the form of liquid (LM) rather than vapor (VM). Allowing vapor to be pulled off the system as product would surely add to the bad reputation of continuous systems not being able to make a good cut. Continuous systems can btw make a cut. Just not as good as a batch system.
But my point here is that measuring the temperature of vapor to make an assumption about collecting product at a specific plate level on a continuous system would be a flawed way to think. Much better off picking a plate level, draw off some product, taste it, then do the same on a different plate level. Once the sampling is complete,,,,pull product from the plate level that renders the desired outcome. Plate temps are nothing more than a by-product, a result of the function. Secondary data at best. Kinda like how the old timers did it.
Also,,, best not to confuse fuel production with spirits production as the OP alluded to in my first observation. Hopefully I don't have to explain why.
Then there is this:
All batch stills starts out with the boiler at a low temperature and works it's way up toward 100C/212F as it's depleted of alcohol. If YOU LEARN by logging where your hearts and tails come off the still, then you most certainly can use that temperature knowledge to your advantage as many of us do this. On a simple pot still for example you can set the target temp where your heads end/hearts start and get a clean transition. If you hold that temp the still will actually stop producing spirit (concentration of heads are taken). Then you can raise the target temp point and pull hearts. If you don't raise this target temperature the still will again slow down and stop producing and you have your hearts. Then when you raise the temperature again by raising your target temperature you will pull the tails. This is simply using the data you've logged in the past for your still to know where to set these target temps. You simply can not pull tails from a pot still if you don't allow the temperature to rise to where they come out!
You just do not need a PID to run this way. Nearly every operator running a little plated column knows that when they dial in their 100% variable SSR controller (or propane valve) and their coolant flow that they can make their still slow down at the end of a perceived cut point.
I mean you can run that way (with a PID),,,,but good grief its just not optimal to allow the PID to shut down the heat input and drop every bit of vapor out of suspension.
So you can certainly create set points if ya like. But if you've read the Methanol write up post above, you should be able to gather that the constituents contained within 100% infinitely miscible solutions very often have boiling points that are so very close (because of homogeneous miscibility) that you'd have to adjust your resolution beyond the capability of a $100.00 PID. In other words, the Amazon PID isn't capable of making a cut based on a predetermined temp setting. The only thing it does is stop your product flow and drop your vapor out of suspension.
Can you run your still with a PID? Sure.
Didn't want to get to the point where folks get undignified or anything. There was definitely some confusion and lack of context (or maybe irrelevant context?) on that thread beyond the PID debate.
Was just looking to politely comment about a couple of talking points used. My comments surely would have pulled the thread into another direction all together.
A really (really, really ) old timer once asked me to only talk about what I know. Hopefully I can articulate?
The first thing to really stick out toward the end of that thread was this:
All fuel and alcohol distillation takes place by temperature. Methanol for example is one of the first things to come off at low temps, followed by other foreshots components, then comes your heads at slightly higher temperatures. Then hearts come off next at higher temperatures, followed by tails. The key being each of these come off at progressively higher temperatures.
Please have a read through this write up to gain a bit more clarity about Methanol:
This next comment is absolutely lacking anything substantive:
Big industrial continuous stills have multiple take-off points at different plate levels to take spirits at temperature. Each plate will have a different temperature. Same concept just handled differently.
Operationally, you can't compare temps on a batch system to temps on a continuous system. Batch system temps are ever changing. Batch temps have to change. No choice.
Continuous systems are tuned to run in steady state. This steady state tuning is entirely predicated upon the fact that an alcoholic(beer) mixture is continuously being fed into the system. At no point is any part of the system EVER depleted of alcohol as long as the system is being fed.
Steady state systems do very well with PIDs controlling various operations. But the one thing PIDs do not control as HDNB mentions is heat input to the system. PIDs (or the like) control pump speeds and coolant flow speeds.
As far as pulling product according to fractions are concerned again this concept is predicated upon a continuous feed of a reliably consistent alcoholic beer mixture. As an aside, product is taken off in the form of liquid (LM) rather than vapor (VM). Allowing vapor to be pulled off the system as product would surely add to the bad reputation of continuous systems not being able to make a good cut. Continuous systems can btw make a cut. Just not as good as a batch system.
But my point here is that measuring the temperature of vapor to make an assumption about collecting product at a specific plate level on a continuous system would be a flawed way to think. Much better off picking a plate level, draw off some product, taste it, then do the same on a different plate level. Once the sampling is complete,,,,pull product from the plate level that renders the desired outcome. Plate temps are nothing more than a by-product, a result of the function. Secondary data at best. Kinda like how the old timers did it.
Also,,, best not to confuse fuel production with spirits production as the OP alluded to in my first observation. Hopefully I don't have to explain why.
Then there is this:
All batch stills starts out with the boiler at a low temperature and works it's way up toward 100C/212F as it's depleted of alcohol. If YOU LEARN by logging where your hearts and tails come off the still, then you most certainly can use that temperature knowledge to your advantage as many of us do this. On a simple pot still for example you can set the target temp where your heads end/hearts start and get a clean transition. If you hold that temp the still will actually stop producing spirit (concentration of heads are taken). Then you can raise the target temp point and pull hearts. If you don't raise this target temperature the still will again slow down and stop producing and you have your hearts. Then when you raise the temperature again by raising your target temperature you will pull the tails. This is simply using the data you've logged in the past for your still to know where to set these target temps. You simply can not pull tails from a pot still if you don't allow the temperature to rise to where they come out!
You just do not need a PID to run this way. Nearly every operator running a little plated column knows that when they dial in their 100% variable SSR controller (or propane valve) and their coolant flow that they can make their still slow down at the end of a perceived cut point.
I mean you can run that way (with a PID),,,,but good grief its just not optimal to allow the PID to shut down the heat input and drop every bit of vapor out of suspension.
So you can certainly create set points if ya like. But if you've read the Methanol write up post above, you should be able to gather that the constituents contained within 100% infinitely miscible solutions very often have boiling points that are so very close (because of homogeneous miscibility) that you'd have to adjust your resolution beyond the capability of a $100.00 PID. In other words, the Amazon PID isn't capable of making a cut based on a predetermined temp setting. The only thing it does is stop your product flow and drop your vapor out of suspension.
Can you run your still with a PID? Sure.
Trample the injured and hurdle the dead.
- Saltbush Bill
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Re: Recent Locked Thread
Thank you for putting some sanity back into this topic Larry.
Re: Recent Locked Thread
Sir, at the risk of offending, any chance the title may of this could be changed and set in BOLD RED LETTERS? This post has completely crushed every pre supposed, or long thought understanding of methanol production through out a distillate production I’ve ever read. I did a title search for methanol and a vast majority encompassed the very paradigms this paper obliterates (completely). I understand the original intent (I read that post) but damn, I’ve never had my understanding of a process so completely unravelled and re-distilled. That’s spoon feeding with a freaking dump truck!!
Edit: Forgot to thank you for the post and the time you took to prepare it.
Edit: Forgot to thank you for the post and the time you took to prepare it.
It seems that discussions about alcohol percentage out of your still are remarkably similar to the MPG of your truck.
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Re: Recent Locked Thread
This needs to be a sticky and part of required reading
Thanks for the time and effort to put this together.
Brilliant
Well done
Thanks for the time and effort to put this together.
Brilliant
Well done
My fekking eyes are bleeding! Installed BS Filters - better! :D
Life has gotten interesting!
Life has gotten interesting!
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Re: Recent Locked Thread
Awesome post. I vote this as the best of 2022. With that, I was recently berated and downvoted to oblivion for posting in the firewater reddit about methanol by telling people not to worry about it and that the only bad thing it does is give you a nasty taste and potential headache.
Now we need one on the difference between cleaning and sanitizing and how you don't need to sanitize like you do beer. Who's going to post that one and compete with Larry for best post of the year?
Now we need one on the difference between cleaning and sanitizing and how you don't need to sanitize like you do beer. Who's going to post that one and compete with Larry for best post of the year?
- Acrylic
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Re: Recent Locked Thread
Thanks for this - printing this and making a few copies to distribute amongst close companions involved in the hobby - We are really appreciative to have found definitive information - a bigger plus is crushing the wrong information supplied by a certain (to remain un-named) YouTube personality
Good judgement comes from experience... And experience? Well, that comes from poor judgement
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Re: Recent Locked Thread
Given that this thread was started 2 years ago shouldn't it be best post of 2020?IMALOSERSCUMBAG wrote: ↑Mon Mar 14, 2022 8:14 am Awesome post. I vote this as the best of 2022. With that, I was recently berated and downvoted to oblivion for posting in the firewater reddit about methanol by telling people not to worry about it and that the only bad thing it does is give you a nasty taste and potential headache.
Now we need one on the difference between cleaning and sanitizing and how you don't need to sanitize like you do beer. Who's going to post that one and compete with Larry for best post of the year?
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Re: Recent Locked Thread
You're never gonna avoid blatant ignorance and gang mentality. Just be glad you didn't make a blasphemous claim of ergot poisoning during the Salem witch trials.IMALOSERSCUMBAG wrote: ↑Mon Mar 14, 2022 8:14 am I was recently berated and downvoted to oblivion for posting in the firewater reddit about methanol by telling people not to worry about it and that the only bad thing it does is give you a nasty taste and potential headache.
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Re: Recent Locked Thread
I can’t believe it sat there for two years without catching fire. I had to read the damn thing four times to make sure I was actually reading and understanding it. NEVER seen it anywhere else. Kinda makes you wonder why…
Best of 2020, 2021, and 2022 in my book. Methanol is THE anchor hanging around the necks of home distillers the world around. I second required reading. Heck if anyone read my posts I’d consider putting a link to it in my sig. At this point, that would be similar to the dustbin of history.
Until it gets a sticky, keep posting and it will stay at the top and maybe even get a hot topic flame thingy.
It seems that discussions about alcohol percentage out of your still are remarkably similar to the MPG of your truck.
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Re: Recent Locked Thread
To be honest, I rarely look at the dates.cranky wrote: ↑Mon Mar 14, 2022 6:19 pmGiven that this thread was started 2 years ago shouldn't it be best post of 2020?IMALOSERSCUMBAG wrote: ↑Mon Mar 14, 2022 8:14 am Awesome post. I vote this as the best of 2022. With that, I was recently berated and downvoted to oblivion for posting in the firewater reddit about methanol by telling people not to worry about it and that the only bad thing it does is give you a nasty taste and potential headache.
Now we need one on the difference between cleaning and sanitizing and how you don't need to sanitize like you do beer. Who's going to post that one and compete with Larry for best post of the year?
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Re: Recent Locked Thread
I should know better myself , but it git me too scumbag .IMALOSERSCUMBAG wrote: ↑Tue Mar 15, 2022 8:21 amTo be honest, I rarely look at the dates.cranky wrote: ↑Mon Mar 14, 2022 6:19 pmGiven that this thread was started 2 years ago shouldn't it be best post of 2020?IMALOSERSCUMBAG wrote: ↑Mon Mar 14, 2022 8:14 am Awesome post. I vote this as the best of 2022. With that, I was recently berated and downvoted to oblivion for posting in the firewater reddit about methanol by telling people not to worry about it and that the only bad thing it does is give you a nasty taste and potential headache.
Now we need one on the difference between cleaning and sanitizing and how you don't need to sanitize like you do beer. Who's going to post that one and compete with Larry for best post of the year?
I was reading back trying to work out which topic had been recently locked .
My recommended goto .
https://homedistiller.org/wiki/index.ph ... ion_Theory
https://homedistiller.org/wiki/index.ph ... ion_Theory
Re: Recent Locked Thread
I dont remember which one exactly yummy. It was one of those many debates about the use of PID for batch distillation.
A relatively new member had basically put far too much stock into what George was preaching.
As I recall the member wasn't taking the info provided here very well and things got heated. So the thread got locked because it turned into more of an argument more than a debate.
A relatively new member had basically put far too much stock into what George was preaching.
As I recall the member wasn't taking the info provided here very well and things got heated. So the thread got locked because it turned into more of an argument more than a debate.
Trample the injured and hurdle the dead.
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Re: Recent Locked Thread
Lol. I started with a PID controller and a stock pot still. That thing smeared like a gopher on the hi-way!LWTCS wrote: ↑Wed Mar 16, 2022 5:50 am I dont remember which one exactly yummy. It was one of those many debates about the use of PID for batch distillation.
A relatively new member had basically put far too much stock into what George was preaching.
As I recall the member wasn't taking the info provided here very well and things got heated. So the thread got locked because it turned into more of an argument more than a debate.
Thanks to HD the PID Is used to run my charcoal smoker.
"What harms us is to persist in self deceit and ignorance"
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Re: Recent Locked Thread
"What harms us is to persist in self deceit and ignorance"
Marcus Aurelius
I’m not an alcoholic! I’m a drunk. Alcoholics go to meetings!
Marcus Aurelius
I’m not an alcoholic! I’m a drunk. Alcoholics go to meetings!
- IMALOSERSCUMBAG
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Re: Recent Locked Thread
Speaking of PID controllers....... Nope, not going there. I'm safer talking about Religion.
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Re: Recent Locked Thread
I'm pretty sure it was this train wreck of a thread by CayersLWTCS wrote: ↑Wed Mar 16, 2022 5:50 am I dont remember which one exactly yummy. It was one of those many debates about the use of PID for batch distillation.
A relatively new member had basically put far too much stock into what George was preaching.
As I recall the member wasn't taking the info provided here very well and things got heated. So the thread got locked because it turned into more of an argument more than a debate.
viewtopic.php?f=85&t=77252
The last page is where the quotes came from
Re: Recent Locked Thread
Ah thanks.cranky wrote: ↑Wed Mar 16, 2022 2:44 pmI'm pretty sure it was this train wreck of a thread by CayersLWTCS wrote: ↑Wed Mar 16, 2022 5:50 am I dont remember which one exactly yummy. It was one of those many debates about the use of PID for batch distillation.
A relatively new member had basically put far too much stock into what George was preaching.
As I recall the member wasn't taking the info provided here very well and things got heated. So the thread got locked because it turned into more of an argument more than a debate.
viewtopic.php?f=85&t=77252
The last page is where the quotes came from
Yeah he (cayers) was another engineer that couldn't make the cross over.
Trample the injured and hurdle the dead.
- cranky
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Re: Recent Locked Thread
So many of George Duncan's disciples couldn't make that cross over.
I was so tempted to buy a PID and video running my 3.5" glass CM the way those guys were claiming how to run it and another showing it running with my SSR but I'm not willing to waste $50 just to prove the point. If my youtube channel was dedicaed to distilling I probably would have.
Re: Recent Locked Thread
I read the original post, I’ve seen the YouTube stuff, been reading here for some time. Don’t know enough to comment on them. All I know is the 8 or 10 people who I showed this information were both surprised and pissed. Most had been sold the same bill o goods. I’m with acrylic, gonna see if the brains of the family can get this printed and passed out. Lots of bulletin boards at grocery stores, co-ops and such. Heck, might even sneak one onto the bulletin board at the sheriff’s office for fun. You just never know who’s gonna read it.
It seems that discussions about alcohol percentage out of your still are remarkably similar to the MPG of your truck.
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Re: Recent Locked Thread
That was indeed a great post and I totally agree.
I think this is an incredibly important topic.
I came to understand it slightly differently and perhaps my explanation might help someone.
Imagine a pot reflux still. The boiler has 10 percent etoh and is boiling. The top of the column is producing 95 percent.
Anywhere on the column in the packing between these two limits is somewhere between 50 and 95 percent Etoh.
The temperature will be between 172 and 195 ish.
Find the temp and you can use the chart to find the etoh concentration.
The chart is magic and very powerful.
Again, I offer this respectfully.
I think this is an incredibly important topic.
I came to understand it slightly differently and perhaps my explanation might help someone.
Imagine a pot reflux still. The boiler has 10 percent etoh and is boiling. The top of the column is producing 95 percent.
Anywhere on the column in the packing between these two limits is somewhere between 50 and 95 percent Etoh.
The temperature will be between 172 and 195 ish.
Find the temp and you can use the chart to find the etoh concentration.
The chart is magic and very powerful.
Again, I offer this respectfully.
Now I know how you claim azeo so easy, it's based on a meat thermometer. :lol:
- Dancing4dan
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Re: Recent Locked Thread
WHAT?drmiller100 wrote: ↑Sun Mar 20, 2022 6:51 pm “Imagine a pot reflux still” …… “ish” …..”The chart is magic and very powerful.”
I have so much more to learn!
"What harms us is to persist in self deceit and ignorance"
Marcus Aurelius
I’m not an alcoholic! I’m a drunk. Alcoholics go to meetings!
Marcus Aurelius
I’m not an alcoholic! I’m a drunk. Alcoholics go to meetings!
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Re: Recent Locked Thread
Lol!!! Yeah, I was being lazy and you caught me!!!!!Dancing4dan wrote: ↑Sun Mar 20, 2022 7:45 pmWHAT?drmiller100 wrote: ↑Sun Mar 20, 2022 6:51 pm “Imagine a pot reflux still” …… “ish” …..”The chart is magic and very powerful.”
I have so much more to learn!
Now I know how you claim azeo so easy, it's based on a meat thermometer. :lol:
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Re: Recent Locked Thread
What is a pot reflux still, its either one or the other imo.
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Re: Recent Locked Thread
I think he means Pot = Batch reflux still. compared to Continuous Stripping + Rectification Still.Saltbush Bill wrote: ↑Sun Mar 20, 2022 8:26 pm What is a pot reflux still, its either one or the other imo.
I say this as someone reading his entire post history trying to learn his knowledge.
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Re: Recent Locked Thread
Sorry. You are right. My mind is wandering tonight.Saltbush Bill wrote: ↑Sun Mar 20, 2022 8:26 pm What is a pot reflux still, its either one or the other imo.
Now I know how you claim azeo so easy, it's based on a meat thermometer. :lol: