40ltr keg, cm still, 2 2000w elements.

Vapor, Liquid or Cooling Management. Flutes, plates, etc.

Moderator: Site Moderator

Post Reply
Ogradygin
Novice
Posts: 3
Joined: Wed Oct 11, 2023 3:26 pm

40ltr keg, cm still, 2 2000w elements.

Post by Ogradygin »

Hi all!
I've been stilling with my 40ltr kegg element boiler
for over a year know,
Still have alot to learn! Loving the art!
I have a question about how to run my still on a neutral sugarwash spirit run.
I have 2 2000w elements one hooked upto a controller,
A 75cm long 2.5inch copper column packed with scrubbies and glass marbles.
Then a 3 inch dephlegmator
Then a 2.5 inch bend
Then my 2.5inch copper shotgun condenser

I'm wanting to know how much power I should be pushing through it when taking off product.
I think I am being abit cautious with how much power I'm running and tend to turn the water flow down on the dephleg more.
I'm still getting 95% the whole way through
I just finding it to be not quite as clean as I expect
And find it difficult to determine between heads hearts and tails.
I take cuts in small 200-400ml jars
And that is with around 35ltrs of 40% low wines in boiler
Should I put a thermometer above my dephlag?/what temperature should I be aiming for? 78°c?

Any help/advice would be much appreciated 😁
MooseMan
Master of Distillation
Posts: 3294
Joined: Fri May 28, 2021 4:54 am
Location: Wales UK

Re: 40ltr keg, cm still, 2 2000w elements.

Post by MooseMan »

I'm at work so I've only skim read this but at 750mm packed length I think you're going to struggle to get it neutral.

I run a 2.5" reflux column and my packed length is 50" whatever that is in mm?
Make Booze, not War!
howie
Trainee
Posts: 786
Joined: Sun Jul 19, 2020 7:34 am

Re: 40ltr keg, cm still, 2 2000w elements.

Post by howie »

i wondered about only 75cm as well, maybe you need at least 1- 1.2m

sounds like it's all smeared if you can't tell heads/hearts/tails, it's quite distinctive if done correctly.
is your column insulated for starters?
do you hold the still in full reflux to stack the fractions, then slowly let the vapors through?
i use a thermometer before the deflag to monitor the temp during the full reflux *, when it drops a couple of degrees, i know the column is stacked.

* = a digital probe thermometer, inserted between column and insulation.

i use a thermometer after the deflag, as well, to do 2 things
1) check that nothing is getting past the deflag during full reflux
2) watch the rise in temp as i reduce the water to deflag to let the top fractions (heads) through, after stacking the column.
drmiller100
Rumrunner
Posts: 694
Joined: Wed Mar 11, 2009 9:13 pm

Re: 40ltr keg, cm still, 2 2000w elements.

Post by drmiller100 »

I never got a column under about 33 inches to run efficiently.
2.5 inch column. I know 2 inch is about 2000 watts. 3 iinch is about 4000 watts.

On a good reflux column on startup it will be just under boiling temp of etoh. That depends on altitude, precision if probe etc. When you pull the heads it may drop a degree or two as the make the mix boil slightly lower.
Now I know how you claim azeo so easy, it's based on a meat thermometer. :lol:
User avatar
Saltbush Bill
Global moderator
Posts: 11641
Joined: Thu Mar 17, 2011 2:13 am
Location: Northern NSW Australia

Re: 40ltr keg, cm still, 2 2000w elements.

Post by Saltbush Bill »

Posting a photo of your still will help get better answers.
User avatar
bunny
Swill Maker
Posts: 412
Joined: Fri Jun 26, 2020 8:28 am

Re: 40ltr keg, cm still, 2 2000w elements.

Post by bunny »

Ogradygin wrote: ↑Tue Oct 17, 2023 4:48 am Hi all!
I've been stilling with my 40ltr kegg element boiler
for over a year know,
Still have alot to learn! Loving the art!
I have a question about how to run my still on a neutral sugarwash spirit run.
I have 2 2000w elements one hooked upto a controller,
A 75cm long 2.5inch copper column packed with scrubbies and glass marbles.
Then a 3 inch dephlegmator
Then a 2.5 inch bend
Then my 2.5inch copper shotgun condenser

I'm wanting to know how much power I should be pushing through it when taking off product.
I think I am being abit cautious with how much power I'm running and tend to turn the water flow down on the dephleg more.
I'm still getting 95% the whole way through
I just finding it to be not quite as clean as I expect
And find it difficult to determine between heads hearts and tails.
I take cuts in small 200-400ml jars
And that is with around 35ltrs of 40% low wines in boiler
Should I put a thermometer above my dephlag?/what temperature should I be aiming for? 78°c?

Any help/advice would be much appreciated 😁
After a year of fighting it you seem to have figured out just how hard a CM setup can be to get what you want. You could keep after it until you are successful (some have :lol: ), or, you could cut your losses and switch to LM, or VM.
I have no doubt you are collecting too fast.

Since you are not happy with the cleanliness of 95% you might keep reading til you find the thread on 97.2% ABV being azeo.

You could start your rebuild by adding a second 75cm x 2.5" column on top of your current column. Fill the 150cm x 2.5" column with scoria or similar appropriate sized lava or Eheim Substrat Pro Pearls made from sintered glass.

Now, if you have enough ceiling clearance, stick a Boka on top and collect some serious neutral.
There are other LM heads with varying amounts of overhead clearance required and a few VM to consider. Overall a change of process will make a huge difference.
Ogradygin
Novice
Posts: 3
Joined: Wed Oct 11, 2023 3:26 pm

Re: 40ltr keg, cm still, 2 2000w elements.

Post by Ogradygin »

Thanks for the input! Yeah I most likely am collecting to fast 😅. Maybe I shouldnt fill my still up so much as the run can drag on for over 12 hours and still be pumping out 95%
I will post up a photo of my set up when I get home tonight 👌 but yes a few upgrades might be on the cards 😁
Post Reply