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First Vapour Management

Posted: Wed Aug 12, 2009 5:32 am
by plonker
I made the mistakes so you dont have to... :ebiggrin:

Design, made mistakes with the length of the take off arm and the diameter of the liebig.
VM design.jpg
If i did it again, I would still use 2" for the column, and 1.5 for the take off, but would bring it down to a liebig 0.75 outer with a 0.5 inner straight after the gate valve. Mine has too much diameter, which form a bit of a suction as the vapour collapses. Occasionally I get a bit of vapour coming out of the liebig coz of the size, but a bit of scrubber sorts that out.

It produces 95.5% throughout all of the heads and hearts. drops to 85% during the tails... If i really push it it will get down to 50%, but its not worth it. I get very little ethanol doing so.. Im very happy with it. Its not fast but its very clean, and as a vodka drinker it prodices wonderful spirit with no hangovers.. :esmile:

Some pics
hmm... unweildy...
hmm... unweildy...
Its pretty tall, I have to tie it to the roof... 25L boiler..
It is all welded but had a little leak that needed solder
It is all welded but had a little leak that needed solder
I wouldn't weld everything again either.. just the vapour take off, at least with solder you can change it later if you want to.
Ready to go...
Ready to go...

Stainless next time, but I AM going to get my value out of that aluminium pot (cost $130 AUS) :shock:
wouldn't use aluminum again.. corrodes to quickly..
wouldn't use aluminum again.. corrodes to quickly..

Re: First Vapour Management

Posted: Wed Aug 12, 2009 5:43 am
by plonker
Cold finger, 1" with 1/4' wrap.. needs a bit of copper wire to get a tight fit.. :D
IMG_2073.JPG
5+ feet of SS scrubbers
IMG_2075.JPG
Gate valve and detachable reflux coil.. works a treat
IMG_2078.JPG
Gate Valve.. was a nightmare to weld.. would get brass fittings and not weld next time... that why my take off arm is too long... :(
IMG_2085.JPG
Doing a run.. works a treat!! :ebiggrin: :ebiggrin: :ebiggrin: