2" bubble cap column add-on
Posted: Fri Mar 26, 2010 3:52 pm
Alright fellas, had some downtime offshore which has let my mind do some wandering. Thinking about adding on a section of 3" packed column downstream of the 2" bubble cap still. The reason for doing so would be to increase output and still maintain 95%. Right now with the bubble cap still I can get around 1/2L per hour. This can make for some long runs. At around 1L per hour the purity drops off to the upper 80's%.
Here's what I'm thinking:
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The bubble cap column is 2" copper. Would probably look at doing the 3" section in stainless. I'm also thinking that this setup would give me two opportunities to pull off heads, once when they leave the 2" column and hopefully condense in the 1-1/4" as the column is initially heating up, then again in the 3" once equilibrium is reached. Is my thinking on that flawed? Would the 3" add-on be a worthwhile endeavor? I do have a tig welder. Assembly would be a piece of cake.
Here's what I'm thinking:

The bubble cap column is 2" copper. Would probably look at doing the 3" section in stainless. I'm also thinking that this setup would give me two opportunities to pull off heads, once when they leave the 2" column and hopefully condense in the 1-1/4" as the column is initially heating up, then again in the 3" once equilibrium is reached. Is my thinking on that flawed? Would the 3" add-on be a worthwhile endeavor? I do have a tig welder. Assembly would be a piece of cake.