HETP - How accurate are Ackland's calcs?
Posted: Thu Nov 21, 2013 1:35 am
Some fairly impressive maths on the parent site from Tony Ackland around column heights, theoretical plates and HETP. I've read through it a number of times and believe I have a good handle on it. I'm embarking on a 2" column keg boiler based rig build, with a boka head to start. So , again I looked at the info in determining the best column height with scrubbers as packing.
Now, I have a T500 - widely regarded as a journeyman's still. I have a pot and reflux head for it, but the factory reflux head output doesn't seem to match Ackland's calculations? It's a 24" height column at 2" in diameter and it will with a very slow takeoff rate produce 93% @ 20 degrees. Typically I run faster than that and get 91% but...
My interpretation of Ackland's calculations implies that 24" of ceramic raschigs/saddles is only 2-3 theoretical HETP, whereas the actual real world output is equivalent to 5-6 HETP. If this is so, wouldn't a say 36" column on the keg boka be sufficient, especially if using scrubbies with a better HETP than raschigs?
I realise there's a few more plates between a 91% and azeotrope output, and i'm happy with anything inbetween. Any reason to make the column higher than 36" though? I have approx. 80" of 2" stainless for the column so plenty of material, but burner, keg, 48" column, 12" head is getting pretty tall for domestic operation !
Now, I have a T500 - widely regarded as a journeyman's still. I have a pot and reflux head for it, but the factory reflux head output doesn't seem to match Ackland's calculations? It's a 24" height column at 2" in diameter and it will with a very slow takeoff rate produce 93% @ 20 degrees. Typically I run faster than that and get 91% but...
My interpretation of Ackland's calculations implies that 24" of ceramic raschigs/saddles is only 2-3 theoretical HETP, whereas the actual real world output is equivalent to 5-6 HETP. If this is so, wouldn't a say 36" column on the keg boka be sufficient, especially if using scrubbies with a better HETP than raschigs?
I realise there's a few more plates between a 91% and azeotrope output, and i'm happy with anything inbetween. Any reason to make the column higher than 36" though? I have approx. 80" of 2" stainless for the column so plenty of material, but burner, keg, 48" column, 12" head is getting pretty tall for domestic operation !