Clarifying rum essence

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Pyewacket
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Clarifying rum essence

Post by Pyewacket »

I have been interested in trying Mashrookie daughter's rum essence for a while. I knew I would have trouble clarifying the essence as reduced syrups are near impossible to strain through coffee filters. I have been putting it off for that reason. I am not a snob, but I prefer to not have a bunch of spent spices floating around in my rum.

I made some modifications to the recipe. Here it is:

3 cups of water
1 cup of brown sugar
1 rounded teaspoon of cinnamon
6 thumb nail sized shavings of orange zest
1.5 tsp of pure vanilla extract
3/4 tsp of pure almond extract
1/2 tsp of ground allspice
1/2 tsp of ground cloves
50 drops of burnt sugar
1.5 cups of high ABV alcohol -- Neutral or rum is fine.

Put all ingredients in a medium sauce pan EXCEPT the vanilla extract, almond extract, burnt sugar, and high ABV alcohol. Bring to a boil stirring often; Reduce by 1/2. You should have roughly 1.5 cups of syrup. I then add the syrup to this contraption.

Made from a mason jar, solder in a couple copper tubes and you are done.

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Top off with you high ABV alcohol. I used 95.5 neutral, so I added 1.5 cups to bring the ABV around 50%. You are aiming for above 40%.

Once you have done that and mixed the alcohol with the syrup well. Screw on the lid and place it in the freezer. This is why you need the ABV of the solution above 40% -- you do not want it to freeze.

Placing it in the freezer allows the particles to settle faster. However, I do not believe it to be essential...so one could just let it set for a while longer. Let this sit UNDISTURBED in the freezer over night. Remove from the freezer carefully and place at the edge of you table/counter.

The crud at the bottom may freeze...so letting it sit on the counter for a bit might help you to start the siphon easier.

The OPEN ended copper tube coming off the top of the mason jar is how you begin the siphon. Gently blowing into the tube forces the essence at the bottom of the jar to flow/climb up the copper tube; if you look close, you can see that I drilled several small holes on the top surface of the tube inside the jar-- I also crimp soldered the end of this tube. This is an easy way to start a siphon without disturbing the sediment crud. That being said, you will of course get a small amount to flow through the holes at the beginning of the siphon. Simply stop the flow by plugging the bottom tube with your finger and dump the first ounce or so...inspect and make sure it is coming out sediment free before you commit to collect the rest.
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Here is what the siphon was able to remove:
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You lose about 3/4 cup of diluted essence -- but well worth it to remove this spent crud.

***EDITED TO ADD: I stopped the siphon a bit early. There were some floaters on the surface that I did not want to collect. Again, just use your finger to plug the take off-- dump the sediment crud.


Now, set up some mason jar coffee filters -- 2 or 3 and run the essence through to remove what the siphon did not. Even with the added alcohol, it can take a couple hours -- so the more filters you set up the better:
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Collect the filtered essence and put it into a medium sauce pan and reduce until all the alcohol is boiled off. ***WARNING*** Even at %40-%50 ABV it can be dangerous to boil off alcohol on a stove top--especially when cooking with an open flame. 1.5 cups of alcohol is plenty enough to cause a fire. Take safety precautions.

Once you have reduced the alcohol off and cooled a bit, add vanilla extract, almond extract, and burnt sugar. You will end up with a rum essence as dark as a dungeon.
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Bagasso
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Re: Clarifying rum essence

Post by Bagasso »

Pyewacket wrote:I knew I would have trouble clarifying the essence as reduced syrups are near impossible to strain through coffee filters.
Boil and filter the spices before adding everything else "EXCEPT the vanilla extract, almond extract, burnt sugar, and high ABV alcohol".
Pyewacket
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Re: Clarifying rum essence

Post by Pyewacket »

If you boil and filter (even if you do not reduce), the filter get plugged full of spice sediment that a couple things happen: 1) you give up. 2) you give up and squeeze the syrup through the coffee filter.

If you squeeze the stuff through, you end up with plenty of cloudy particles. This is my experience with this recipe.

Diluting, and racking out the sediment makes for a nice clear essence. I have tried to pre-filter it in a cotton cloth and than run through the filter...works better but still clogs the coffee filter- and a lot of the smaller particles will pass through.

Is it that important to make a clear essence? Since a bit of spice residue doesn't change the flavor of your spirit, only people touched in the brain with the obsessive gene will care. Just tossing this out as an idea...works for me.
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T-Pee
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Re: Clarifying rum essence

Post by T-Pee »

Isn't that what the gaps between your teeth are for?

tp
Pyewacket
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Joined: Sat Jun 30, 2012 5:49 pm
Location: PAC NW

Re: Clarifying rum essence

Post by Pyewacket »

T-Pee wrote:Isn't that what the gaps between your teeth are for?

tp

LOL indeed
Bagasso
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Re: Clarifying rum essence

Post by Bagasso »

Pyewacket wrote:If you boil and filter (even if you do not reduce), the filter get plugged full of spice sediment that a couple things happen: 1) you give up. 2) you give up and squeeze the syrup through the coffee filter.
No, boil the spices in just water, filter the spices out and then make up the syrup and reduce to where you want it.
Pyewacket
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Re: Clarifying rum essence

Post by Pyewacket »

Interesting idea. I guess I always assumed the magic in flavoring a syrup (like in this recipe) was the interaction that occurs with the boil. Sugar and water starts boiling at roughly 212degs, and as the syrup reduces the temperature climbs. For the 20mins it takes to reduce this recipe -- it spends all of its time climbing between 212-275degs F. I also assumed that the the aggressively osmotic/diffusive forces of the sugar works to further draw out the essence of the spices -- while boiling and while resting. For example, when you remove the orange zest it is completely candied -- dark as the syrup. The cells have become saturated as they have either burst from the heat, or pickled through diffusive forces.

It would probably require recipe overhaul...not sure. To be honest, I'm may be curious enough to try.

But in the end, I would probably still rack the water/spice solution just the same. Filtering works well, but there are always small particles that will find their way through. So if you pour a mucky solution into the filters, you are going to get a certain percentage of pass-through. If you simply rack it first, you will still get a percentage of pass-through -- but since you removed 99% of the sediment...I am going to guess you will get a cleaner result.

The only other issue is the that the sugar tends to interact with the oils and water solubles. This produces a dark slime that sort of congeals on the surface, easily removed during the racking process-- probably just as easy to remove by skimming..
Bagasso
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Re: Clarifying rum essence

Post by Bagasso »

Pyewacket wrote:I also assumed that the the aggressively osmotic/diffusive forces of the sugar works to further draw out the essence of the spices -- while boiling and while resting.
Could be true for whole spices but powdered? I' don't think you need much to draw out flavors from particles the size of flour.

So maybe:
Ground spices with just water = easy filtering

Whole spices with the syrup = easier filtering

Easy being relative of course.
Pyewacket
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Re: Clarifying rum essence

Post by Pyewacket »

Could be fun experimenting with this. I will say that I felt the need to up the spices from the original because when you remove the particles you lose some flavor. And when you boil, the aromatics escape as well. Maybe a hybrid...crushing allspice and cloves would be the best of both worlds.

Again, would have to play around with this and develop a new recipe. Maybe this weekend I will buy some whole spices and try a water boil. Start with a couple tsp of each, crush and boil in water. If the particles that the boil creates stay large -- no need for racking. There is a good chance that the boil will generate sediment and sludge; silty sediment passes though my coffee filter. If that is the case, there is zero reason not to put it in the jar and rack first.

4 cups of water, crushed spices including orange, boil down to 3cups. Large screen filter out the solids, and see what is left. Pour it into the mason jar and let sit. Clear it. Mix with sugar and reduce -- add extracts once cooled...something like this.

The only way to tell if you can get enough flavor is to try it. A combination of these ideas could yield a very clean sediment free essence.
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