I disagree.drmiller100 wrote: ↑Sun Sep 24, 2023 8:28 pm
I believe the way to concentrate the heads is to run it in full reflux a while. Then pull everything off the top on one dump. Should be a table spoon or two.
repeat.
Repeat a third time. If it is still nasty you can go again.
Or. You can pull heads one drop at a time so the nasties get diluted with good etoh.
Sounds like a lot of unneeded fiddling with the take-off vs power balance.
I believe in the slow and steady approach to remove fore shots and heads.
Here's another way to getter done.
18ish gallon pot, with a 4" packed column.
Heat the boiler like you're doing a potstill run.
Set the take off to a fast drip and wait.
During the time it takes to draw off the foreshots, the entire boiler charge will have time to come up to temp and the most volatile nasties will have gotten hot enough to boil off.
Next adjust the take off for a broken stream for the "guestimanted" heads cut.
Last is the hearts setting @ around 3 to 4 ltrs/hour.
As the run progresses the takeoff rate will decrease.
When tails appear shut off the power, drain and clean.