vercingetoriX26 wrote: ↑Thu Dec 14, 2023 12:48 am
Next did a spirit run and broke it into 6 glass jars.
Jar 1: Temp 78-81 degrees; ABV=70%
Jar 2: Temp 81-82 degrees; ABV= 80%
Jar 3: Temp 82-86 degrees; ABV= 80 to 73%
Jar 4: Temp 85-89 degrees; ABV= 75 to 60%
Jar 5: Temp 89-94 degrees; ABV= 60 to 40%
Jar 6: Temp 92-96 degrees; ABV= 39 to 20%
To my amateur palette, neither of the jars taste/smell noticeably different (aside from obvious ABV) to suggest that either Jar 1 contains acetone or that Jar 6 contains nasty fusel oils.
OK, as a rum “newbie”, making cuts on a rum is challenging for sure. So, help yourself by making a “finer comb”, that is, more collection jars. More jars will help you identify the changes as you smell and taste your way through them to choose the “good from the bad”. You’ll also be able to train your palette for these subtleties. Experience will teach you a lot.
What I would do is
keep jar 3 as a “white stash” for sipping as an inspiration.
And take the rest (jars 1 &2, and 4, 5, and 6) and RERUN it through the still. You may need to dilute it with water to get it back to 40%ABV, but you may be close without dilution. Then, and this is important …
collect into 15 to 20 jars … you should have a pretty good idea how much your total volume will be, so just divide that by 15 and that’s roughly how much each jar should collect before changing jars.
Rerunning will help refine the collection of jars you have and it will allow you better separation between jars such that you’ll be able to discern the difference between one end of the collection from the other. More jars will help you with the “gradient” of the product as it comes offstill.
vercingetoriX26 wrote: ↑Thu Dec 14, 2023 12:48 am… Is it therefore necessary to toss out Jars 1 and 6 as Heads & Tails?
I wouldn’t “toss out” these jars, but you should get MORE jars. Six jars is NOT ENOUGH to make good cuts unless you made this product “umpteen times” such that you KNOW how much is hearts and how much is not.
Running a still is an “art”, so keep practicing. Soon, it’ll become 2nd nature and making cuts won’t be a dreaded task, but rather an enjoyable challenge to your ultimate rewards.
ss