distillate coming out cloudy

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mgman71
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Posts: 26
Joined: Fri Aug 17, 2007 5:28 pm
Location: Ontario, Canada

distillate coming out cloudy

Post by mgman71 »

hey guys, i've been distilling for awhile, just finished doing a stripping run and started the final though the reflux column. Problem is the alcohol in the collection container is slightly cloudy! I've never had that happen before. I pack the column with raschig rings, i loaded in some new ones this time but forgot to wash them first... i'm thinking that might be why, any other suggestions? I dumped everything back in and going to start again on the weekend.
kiwistiller
retired
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Joined: Tue Mar 03, 2009 4:09 pm
Location: Auckland, NZ

Re: distillate coming out cloudy

Post by kiwistiller »

could be a) you flooded the column and the still puked
b) you're dragging tails over, or
c) there is crap / dirt / generally nastiness in your still.

by the by, stainless or copper mesh will give you better results as packing :D
Three sheets to the wind!
My stuff
mgman71
Novice
Posts: 26
Joined: Fri Aug 17, 2007 5:28 pm
Location: Ontario, Canada

Re: distillate coming out cloudy

Post by mgman71 »

hmmmm, i think you might be right about the puking, i may have it to full
kiwistiller
retired
Posts: 3215
Joined: Tue Mar 03, 2009 4:09 pm
Location: Auckland, NZ

Re: distillate coming out cloudy

Post by kiwistiller »

if it was puking, you'd have noticed a sudden increase in collection, and possibly gurgling noises coming from the column. ring any bells?
Three sheets to the wind!
My stuff
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