Burbon Recipe into 3 gal barrel for 20 months (bad outcome)

Treatment and handling of your distillate.

Moderator: Site Moderator

Post Reply
theskaz
Novice
Posts: 98
Joined: Tue Jan 19, 2016 12:59 pm

Burbon Recipe into 3 gal barrel for 20 months (bad outcome)

Post by theskaz »

Recipe thread:

viewtopic.php?f=3&t=65138

it's been 20 months since the barrel has been sealed and we decided to empty it a couple days ago. We opened it a month in, a year in, and 15 months in to test it out.

the spirits got real "hot" about a month after putting it in the barrel, and never let up. I think 20 months was waaay too long and I dont like this stuff. throwing ice on it makes it tolerable. Looking for a post mortem to find out where I went wrong.

also, for that length of time, i got 1.2 gallons out of the 3 gallon barrel. I watered it down to 80 proof trying to take some of the fire out. it worked a little. Im sure there are more details you all need, just let me know what that might be, and Ill do what I can to answer them.
20181031_122850.jpg
20181031_122859.jpg
theskaz
Novice
Posts: 98
Joined: Tue Jan 19, 2016 12:59 pm

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by theskaz »

it tastes like cherry(?)/vanilla flavored gasoline
User avatar
ShineonCrazyDiamond
Global moderator
Posts: 3468
Joined: Thu Feb 27, 2014 6:14 pm
Location: Look Up

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by ShineonCrazyDiamond »

Put it im the closet and forget about it for 2 weeks. It needs time to stabilize.
"Come on you stranger, you legend, you martyr, and shine!
You reached for the secret too soon, you cried for the moon.
Shine on you crazy diamond."
theskaz
Novice
Posts: 98
Joined: Tue Jan 19, 2016 12:59 pm

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by theskaz »

no problem! i was wondering if that would help.
User avatar
kiwi Bruce
Distiller
Posts: 2451
Joined: Mon Apr 23, 2012 12:38 pm
Location: Transplanted Kiwi living in the States

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by kiwi Bruce »

How did you do your cuts? What was the strength going into the barrel? and was the barrel new or used oak?
All that fun we had growing up...We pay for as we grow old.
User avatar
JellybeanCorncob
Swill Maker
Posts: 485
Joined: Thu Mar 12, 2015 7:18 am
Location: Under the Redwood Trees

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by JellybeanCorncob »

180 proof into the barrel?
Waaa?
JBC
JBC
User avatar
HDNB
Site Mod
Posts: 7427
Joined: Mon Feb 17, 2014 10:04 am
Location: the f-f-fu frozen north

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by HDNB »

JellybeanCorncob wrote:180 proof into the barrel?
Waaa?
JBC
i had to go find this.

"I have about 2.5 gallons of 180 proof goodness to go into my 3 gallon barrel. i didnt get much into the heads or tails. Im wondering if pulling some hearts out to add a little tail, or just leave it all hearts and let it age... cuts is something im still stupid on. hard to get an idea of what it will taste like after it ages when you are doing cuts."


i think all of your problems are right there in that sentence. bads cuts, aging hi proof vodka.

live and learn. hope you have been making more and better while the last 20 montrhs flashed by.
I finally quit drinking for good.

now i drink for evil.
StillerBoy
Master of Distillation
Posts: 3387
Joined: Thu Dec 01, 2016 6:27 pm
Location: Ontario

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by StillerBoy »

HDNB wrote:live and learn. hope you have been making more and better while the last 20 montrhs flashed by.
+1

Has not yet learn, because he's asking what happen.. Who in his right mind would put 180 proof on oak.. need much reading and comprehend yet..

Mars
" I know quite certainly that I myself have no special talent. Curiosity, Obsession and dogged endurance, combined with self-criticism, have brought me to my knowledge and understanding "

– Albert Einstein
User avatar
NZChris
Master of Distillation
Posts: 13924
Joined: Tue Apr 23, 2013 2:42 am
Location: New Zealand

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by NZChris »

Put some new make in the barrel in the low 120s and use that for blending with your first run after a few months.

If you are in a hurry, some new make might make an ok blend straight away or given a few weeks to settle down in a jar with some headspace for O2.

A couple of your comments make me wonder if you think it should taste ok at very high abvs. If that is the case, someone has been feeding you misinformation.
OtisT
Master of Distillation
Posts: 3322
Joined: Sat Oct 24, 2015 11:59 am
Location: Pacific Northwest

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by OtisT »

In addition to needing a lower AVB and better cuts, also consider that a 3 gal barrel has a high wood area to liquid volume ratio compared to larger barrels, so you should not expect to soak as long as a larger barrel to get enough oak.

Otis
Otis’ Pot and Thumper, Dimroth Condenser: Pot-n-Thumper/Dimroth
Learning to Toast: Toasting Wood
Polishing Spirits with Fruitwood: Fruitwood
Badmotivator’s Barrels: Badmo Barrels
User avatar
kiwi Bruce
Distiller
Posts: 2451
Joined: Mon Apr 23, 2012 12:38 pm
Location: Transplanted Kiwi living in the States

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by kiwi Bruce »

theskaz other than a loss of time, chalk this up and learn from it...the cuts are critical, go back and read, read, read some more...and better luck next time...+1 Otis T and NZ Chris
All that fun we had growing up...We pay for as we grow old.
User avatar
still_stirrin
Master of Distillation
Posts: 10372
Joined: Tue Mar 18, 2014 7:01 am
Location: where the buffalo roam, and the deer & antelope play

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by still_stirrin »

theskaz wrote:...i got 1.2 gallons out of the 3 gallon barrel. I watered it down to 80 proof trying to take some of the fire out. it worked a little...
What was the %ABV of the 1.2 gallons you got out of the 3 gallon cask? 90%ABV into the cask and ??? out? Did it go down, or up?

You said you tempered it down to 80 proof (40%ABV) and it’s still “hot”. That sounds like the solvents in the heads. Often those are quite volatile...to the extent that they will evaporate off first. But diluting the spirit will obviously retard that process.

Possibly the best way to save it is to rerun it. Or, like NZChris suggested....blend it into something good. But if it is truly “off the mark” and can’t be made drinkable, rerunning it will salvage some of it.

Unfortunately, sometimes lessons are learned the hard way....through time. You can’t turn back the clock, but you can get aonther chance to do it properly...especially now that you’re more experienced.
ss
My LM/VM & Potstill: My build thread
My Cadco hotplate modification thread: Hotplate Build
My stock pot gin still: stock pot potstill
My 5-grain Bourbon recipe: Special K
User avatar
HDNB
Site Mod
Posts: 7427
Joined: Mon Feb 17, 2014 10:04 am
Location: the f-f-fu frozen north

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by HDNB »

2.5 gallons in at 180 would strip tannins but no sugar. 20 months later and reduced by 1.3 gallons you would have 1.2gal of very concentrated tincture of oak, with no wood sugars dissolved into the mix.

bitter, astringent firewater would be my imagined outcome. Thanks for sharing...one lesson i won't try to duplicate.

I like NZC's solution, blend with a lower proof (or water) and get some wood sugars dissolved in and it would likely (hopefully?) turn a corner.
I finally quit drinking for good.

now i drink for evil.
User avatar
kiwi Bruce
Distiller
Posts: 2451
Joined: Mon Apr 23, 2012 12:38 pm
Location: Transplanted Kiwi living in the States

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by kiwi Bruce »

Would it be possible to add xylose to get the wood sugar level back?
All that fun we had growing up...We pay for as we grow old.
theskaz
Novice
Posts: 98
Joined: Tue Jan 19, 2016 12:59 pm

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by theskaz »

I didnt realize there were any more replies to this.

I did not put the stuff in there at 180 proof. I did it at 125. as far as cuts, i tend to leave out a good chunk of the heads, and will go into tails a bit.
theskaz
Novice
Posts: 98
Joined: Tue Jan 19, 2016 12:59 pm

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by theskaz »

i have 1 quart of hearts from the original run @ 180 proof, I have that at my disposal. It went in @ 125 proof, and came out @ 112. then watered it down to 80 at this point.
User avatar
JellybeanCorncob
Swill Maker
Posts: 485
Joined: Thu Mar 12, 2015 7:18 am
Location: Under the Redwood Trees

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by JellybeanCorncob »

Theskaz: So you ran this through a bokabob and your hearts were 90% ABV? That’s vodka. No flavor there right? I think you said you added no heads at all? And you blended tales, yet you don’t fully understand how to make cuts? Hmmm. I hope you’ve learned the basics in the past 20 months. In my opinion it is Imperative that they are learned and practiced. If for nothing else for safety, let alone a quality liquor.
I’m not trying to piss you off. I’m truly concerned.
Good luck to you.
Take care.
JBC
JBC
User avatar
kiwi Bruce
Distiller
Posts: 2451
Joined: Mon Apr 23, 2012 12:38 pm
Location: Transplanted Kiwi living in the States

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by kiwi Bruce »

JellybeanCorncob wrote: I hope you’ve learned the basics in the past 20 months. In my opinion it is Imperative that they are learned and practiced.
+1...I agree
All that fun we had growing up...We pay for as we grow old.
theskaz
Novice
Posts: 98
Joined: Tue Jan 19, 2016 12:59 pm

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by theskaz »

Ill totally chalk it up to a learning experience, i have no problem with that. that being said, I have to learn, so... what all went wrong?

Most of my posts are very short, as to just get to the point, but i will go in further detail to try and snuff out errors.

what I am hearing, is that even though I used a bourbon recipe, because i used a reflux still, I still got vodka. I know that refluxing will create a more neutral product, But vodka wasnt my goal. My thoughts were that If the product was more neutral, it will pull more flavors from the barrel. this comes from a couple guesses, and 1 successful run.

I had a 10 gallon barrel that I did All grain, 2 row. I used the same still, the same process. and put 10 gallons in for about a year. Out of that came one of the best "whiskeys" I have ever tasted.

I took that and tried to make a more traditional (without building another still) bourbon. smaller batch, didnt think i needed to age it as long. goal was 8-10 months. we just couldnt get the fire down. so figured it needed to sit longer.
i had a 30Gal fermentor and split into 2 runs. i divvied up the run into 1qt jars. after the run was over, i took a large stock pot and started from the middle of each run and poured it in. working my way out and leaned toward the tails. I sampled each jar by just putting it on my tongue, and f I didnt like it, it didnt go in. then that was proofed down to 125, and went in the barrel.



so, as far as the post-mortem, I did the following (correct where needed)
1. used a reflux still/I made vodka thinking I made burbon.
2. aged too long
3. cuts?
User avatar
NZChris
Master of Distillation
Posts: 13924
Joined: Tue Apr 23, 2013 2:42 am
Location: New Zealand

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by NZChris »

theskaz wrote:so, as far as the post-mortem, I did the following (correct where needed)
1. used a reflux still/I made vodka thinking I made burbon.
2. aged too long
3. cuts?
1 & 3. At 180 proof I doubt you would have made vodka unless you really badly stuffed up 3.

2. Aged too long in a small wooden barrel. The barrel is partly 'broken in' now, so keep using it.
Don't re-run this batch. That is probably the worst way to fix it because it wastes much of the age it has acquired. Instead, try blends of new make and shorter aged product, continuing to age them in 2/3rds full glassware or SS with a small charred and toasted oak domino to maintain some wood contact. I've got product that I have deliberately over-oaked to damned near black that I use to make very nice blends with other batches, younger and older, and I've got no doubt yours could be used for the same purpose.
Celis
Novice
Posts: 33
Joined: Wed Feb 28, 2018 1:38 am

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by Celis »

Maybe I read I wrong, but did you make cuts by tasting the jars without proofing it down to around 60 proof? I doubt if you can make good cuts at such a high proof.

Regarding the over oaking, don't worry it can still turn out fine. I had some ryebread whiskey with way too much oak and after taking one stick out and leaving the other in, it came around eventually. :)
theskaz
Novice
Posts: 98
Joined: Tue Jan 19, 2016 12:59 pm

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by theskaz »

NZChris wrote:
theskaz wrote:so, as far as the post-mortem, I did the following (correct where needed)
1. used a reflux still/I made vodka thinking I made burbon.
2. aged too long
3. cuts?
1 & 3. At 180 proof I doubt you would have made vodka unless you really badly stuffed up 3.

2. Aged too long in a small wooden barrel. The barrel is partly 'broken in' now, so keep using it.
Don't re-run this batch. That is probably the worst way to fix it because it wastes much of the age it has acquired. Instead, try blends of new make and shorter aged product, continuing to age them in 2/3rds full glassware or SS with a small charred and toasted oak domino to maintain some wood contact. I've got product that I have deliberately over-oaked to damned near black that I use to make very nice blends with other batches, younger and older, and I've got no doubt yours could be used for the same purpose.
That sounds very reasonable. so i am clear, are you saying that the glassware would also have a domino in it? or only with SS? I have a couple 2.5 Gal glass jars that being used right now, but they will be empty shortly. in the mean time, I need to make some more wash.
theskaz
Novice
Posts: 98
Joined: Tue Jan 19, 2016 12:59 pm

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by theskaz »

Celis wrote:Maybe I read I wrong, but did you make cuts by tasting the jars without proofing it down to around 60 proof? I doubt if you can make good cuts at such a high proof.

Regarding the over oaking, don't worry it can still turn out fine. I had some ryebread whiskey with way too much oak and after taking one stick out and leaving the other in, it came around eventually. :)
Cuts are going to be my weakest link. I've done it a dozen times with only the research that is on this site. taking text from posts, and applying it is something I am still working on. I figured that if it hits the tongue and I am pleased, it goes in. if it is full proof, its just going to get better when abv is dropped.

I would love to get better at this, but that is going to be experience at this point, unless someone wants to come to the bottom left corner of the US and do a run with me :) I do maybe a couple runs a year.
OtisT
Master of Distillation
Posts: 3322
Joined: Sat Oct 24, 2015 11:59 am
Location: Pacific Northwest

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by OtisT »

theskaz wrote:Cuts are going to be my weakest link. I've done it a dozen times with only the research that is on this site. taking text from posts, and applying it is something I am still working on. I figured that if it hits the tongue and I am pleased, it goes in. if it is full proof, its just going to get better when abv is dropped.
You really need to proof it down to taste it and to avoid damaging the tissue in your mouth. You don’t need to proof down the whole jar. Just a small sample. I use a glass eye dropper with 1/10 ml markings on it, others use small glass tubes, etc.

There is a thread “Novice Guide For Cuts” by kiwistiller you should read. Since you are not proofing it down, I am guessing you have not read that one. It’s well worth your time.

Otis
Otis’ Pot and Thumper, Dimroth Condenser: Pot-n-Thumper/Dimroth
Learning to Toast: Toasting Wood
Polishing Spirits with Fruitwood: Fruitwood
Badmotivator’s Barrels: Badmo Barrels
Smokee
Swill Maker
Posts: 241
Joined: Wed Jan 01, 2014 1:35 pm

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by Smokee »

I would throw that back in the still, dilute to 40% and rerun it. Maybe do another few gallons of mash and strip it, add it into the diluted stuff you're going to run again. Then, take your time and do some really good cuts then back in the barrel. Don't let it on wood as long.
User avatar
TDick
Distiller
Posts: 1365
Joined: Thu Jun 01, 2017 9:25 pm
Location: Sweet Home

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by TDick »

theskaz wrote:
Cuts are going to be my weakest link. I've done it a dozen times with only the research that is on this site. taking text from posts, and applying it is something I am still working on. I figured that if it hits the tongue and I am pleased, it goes in. if it is full proof, its just going to get better when abv is dropped.
I'm going to weigh in just a little since you seem to have more experience than me.

Also, here is a youtube video - hold up @Jes2XU is a fellow HD member.
This is a video he did making cuts and appears to be following @Kiwistiller 's guide.
Maybe this will help you visualize the process.



Good luck!
theskaz
Novice
Posts: 98
Joined: Tue Jan 19, 2016 12:59 pm

Re: Burbon Recipe into 3 gal barrel for 20 months (bad outco

Post by theskaz »

Thank you for that, ive watched half of his videos so far.
Post Reply