Recent Locked Thread

Distillation methods and improvements.

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LWTCS
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Recent Locked Thread

Post by LWTCS »

Hey gang,
Didn't want to get to the point where folks get undignified or anything. There was definitely some confusion and lack of context (or maybe irrelevant context?) on that thread beyond the PID debate.
Was just looking to politely comment about a couple of talking points used. My comments surely would have pulled the thread into another direction all together.
A really (really, really :D ) old timer once asked me to only talk about what I know. Hopefully I can articulate?

The first thing to really stick out toward the end of that thread was this:
All fuel and alcohol distillation takes place by temperature. Methanol for example is one of the first things to come off at low temps, followed by other foreshots components, then comes your heads at slightly higher temperatures. Then hearts come off next at higher temperatures, followed by tails. The key being each of these come off at progressively higher temperatures.

Please have a read through this write up to gain a bit more clarity about Methanol:

This next comment is absolutely lacking anything substantive:
Big industrial continuous stills have multiple take-off points at different plate levels to take spirits at temperature. Each plate will have a different temperature. Same concept just handled differently.


Operationally, you can't compare temps on a batch system to temps on a continuous system. Batch system temps are ever changing. Batch temps have to change. No choice.
Continuous systems are tuned to run in steady state. This steady state tuning is entirely predicated upon the fact that an alcoholic(beer) mixture is continuously being fed into the system. At no point is any part of the system EVER depleted of alcohol as long as the system is being fed.
Steady state systems do very well with PIDs controlling various operations. But the one thing PIDs do not control as HDNB mentions is heat input to the system. PIDs (or the like) control pump speeds and coolant flow speeds.

As far as pulling product according to fractions are concerned again this concept is predicated upon a continuous feed of a reliably consistent alcoholic beer mixture. As an aside, product is taken off in the form of liquid (LM) rather than vapor (VM). Allowing vapor to be pulled off the system as product would surely add to the bad reputation of continuous systems not being able to make a good cut. Continuous systems can btw make a cut. Just not as good as a batch system.
But my point here is that measuring the temperature of vapor to make an assumption about collecting product at a specific plate level on a continuous system would be a flawed way to think. Much better off picking a plate level, draw off some product, taste it, then do the same on a different plate level. Once the sampling is complete,,,,pull product from the plate level that renders the desired outcome. Plate temps are nothing more than a by-product, a result of the function. Secondary data at best. Kinda like how the old timers did it.
Also,,, best not to confuse fuel production with spirits production as the OP alluded to in my first observation. Hopefully I don't have to explain why.


Then there is this:
All batch stills starts out with the boiler at a low temperature and works it's way up toward 100C/212F as it's depleted of alcohol. If YOU LEARN by logging where your hearts and tails come off the still, then you most certainly can use that temperature knowledge to your advantage as many of us do this. On a simple pot still for example you can set the target temp where your heads end/hearts start and get a clean transition. If you hold that temp the still will actually stop producing spirit (concentration of heads are taken). Then you can raise the target temp point and pull hearts. If you don't raise this target temperature the still will again slow down and stop producing and you have your hearts. Then when you raise the temperature again by raising your target temperature you will pull the tails. This is simply using the data you've logged in the past for your still to know where to set these target temps. You simply can not pull tails from a pot still if you don't allow the temperature to rise to where they come out!

You just do not need a PID to run this way. Nearly every operator running a little plated column knows that when they dial in their 100% variable SSR controller (or propane valve) and their coolant flow that they can make their still slow down at the end of a perceived cut point.
I mean you can run that way (with a PID),,,,but good grief its just not optimal to allow the PID to shut down the heat input and drop every bit of vapor out of suspension.

So you can certainly create set points if ya like. But if you've read the Methanol write up post above, you should be able to gather that the constituents contained within 100% infinitely miscible solutions very often have boiling points that are so very close (because of homogeneous miscibility) that you'd have to adjust your resolution beyond the capability of a $100.00 PID. In other words, the Amazon PID isn't capable of making a cut based on a predetermined temp setting. The only thing it does is stop your product flow and drop your vapor out of suspension.

Can you run your still with a PID? Sure.
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Saltbush Bill
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Re: Recent Locked Thread

Post by Saltbush Bill »

Thank you for putting some sanity back into this topic Larry. :thumbup:
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Re: Recent Locked Thread

Post by Wyododge »

Sir, at the risk of offending, any chance the title may of this could be changed and set in BOLD RED LETTERS? This post has completely crushed every pre supposed, or long thought understanding of methanol production through out a distillate production I’ve ever read. I did a title search for methanol and a vast majority encompassed the very paradigms this paper obliterates (completely). I understand the original intent (I read that post) but damn, I’ve never had my understanding of a process so completely unravelled and re-distilled. That’s spoon feeding with a freaking dump truck!!

Edit: Forgot to thank you for the post and the time you took to prepare it.
It seems that discussions about alcohol percentage out of your still are remarkably similar to the MPG of your truck.
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Re: Recent Locked Thread

Post by EricTheRed »

This needs to be a sticky and part of required reading

Thanks for the time and effort to put this together.
Brilliant
Well done
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Re: Recent Locked Thread

Post by IMALOSERSCUMBAG »

Awesome post. I vote this as the best of 2022. With that, I was recently berated and downvoted to oblivion for posting in the firewater reddit about methanol by telling people not to worry about it and that the only bad thing it does is give you a nasty taste and potential headache.

Now we need one on the difference between cleaning and sanitizing and how you don't need to sanitize like you do beer. Who's going to post that one and compete with Larry for best post of the year?
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Re: Recent Locked Thread

Post by Acrylic »

Thanks for this - printing this and making a few copies to distribute amongst close companions involved in the hobby - We are really appreciative to have found definitive information - a bigger plus is crushing the wrong information supplied by a certain (to remain un-named) YouTube personality
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Re: Recent Locked Thread

Post by cranky »

IMALOSERSCUMBAG wrote: Mon Mar 14, 2022 8:14 am Awesome post. I vote this as the best of 2022. With that, I was recently berated and downvoted to oblivion for posting in the firewater reddit about methanol by telling people not to worry about it and that the only bad thing it does is give you a nasty taste and potential headache.

Now we need one on the difference between cleaning and sanitizing and how you don't need to sanitize like you do beer. Who's going to post that one and compete with Larry for best post of the year?
Given that this thread was started 2 years ago shouldn't it be best post of 2020?
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Re: Recent Locked Thread

Post by Twisted Brick »

IMALOSERSCUMBAG wrote: Mon Mar 14, 2022 8:14 am I was recently berated and downvoted to oblivion for posting in the firewater reddit about methanol by telling people not to worry about it and that the only bad thing it does is give you a nasty taste and potential headache.
You're never gonna avoid blatant ignorance and gang mentality. Just be glad you didn't make a blasphemous claim of ergot poisoning during the Salem witch trials.
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Re: Recent Locked Thread

Post by Wyododge »

cranky wrote: Mon Mar 14, 2022 6:19 pm Given that this thread was started 2 years ago shouldn't it be best post of 2020?
I can’t believe it sat there for two years without catching fire. I had to read the damn thing four times to make sure I was actually reading and understanding it. NEVER seen it anywhere else. Kinda makes you wonder why…

Best of 2020, 2021, and 2022 in my book. Methanol is THE anchor hanging around the necks of home distillers the world around. I second required reading. Heck if anyone read my posts I’d consider putting a link to it in my sig. At this point, that would be similar to the dustbin of history.

Until it gets a sticky, keep posting and it will stay at the top and maybe even get a hot topic flame thingy.
It seems that discussions about alcohol percentage out of your still are remarkably similar to the MPG of your truck.
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Re: Recent Locked Thread

Post by IMALOSERSCUMBAG »

cranky wrote: Mon Mar 14, 2022 6:19 pm
IMALOSERSCUMBAG wrote: Mon Mar 14, 2022 8:14 am Awesome post. I vote this as the best of 2022. With that, I was recently berated and downvoted to oblivion for posting in the firewater reddit about methanol by telling people not to worry about it and that the only bad thing it does is give you a nasty taste and potential headache.

Now we need one on the difference between cleaning and sanitizing and how you don't need to sanitize like you do beer. Who's going to post that one and compete with Larry for best post of the year?
Given that this thread was started 2 years ago shouldn't it be best post of 2020?
To be honest, I rarely look at the dates.
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Re: Recent Locked Thread

Post by Yummyrum »

IMALOSERSCUMBAG wrote: Tue Mar 15, 2022 8:21 am
cranky wrote: Mon Mar 14, 2022 6:19 pm
IMALOSERSCUMBAG wrote: Mon Mar 14, 2022 8:14 am Awesome post. I vote this as the best of 2022. With that, I was recently berated and downvoted to oblivion for posting in the firewater reddit about methanol by telling people not to worry about it and that the only bad thing it does is give you a nasty taste and potential headache.

Now we need one on the difference between cleaning and sanitizing and how you don't need to sanitize like you do beer. Who's going to post that one and compete with Larry for best post of the year?
Given that this thread was started 2 years ago shouldn't it be best post of 2020?
To be honest, I rarely look at the dates.
I should know better myself , but it git me too scumbag .
I was reading back trying to work out which topic had been recently locked . :oops:
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Re: Recent Locked Thread

Post by LWTCS »

I dont remember which one exactly yummy. It was one of those many debates about the use of PID for batch distillation.
A relatively new member had basically put far too much stock into what George was preaching.

As I recall the member wasn't taking the info provided here very well and things got heated. So the thread got locked because it turned into more of an argument more than a debate.
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Re: Recent Locked Thread

Post by Dancing4dan »

LWTCS wrote: Wed Mar 16, 2022 5:50 am I dont remember which one exactly yummy. It was one of those many debates about the use of PID for batch distillation.
A relatively new member had basically put far too much stock into what George was preaching.

As I recall the member wasn't taking the info provided here very well and things got heated. So the thread got locked because it turned into more of an argument more than a debate.
Lol. I started with a PID controller and a stock pot still. :crazy: That thing smeared like a gopher on the hi-way!

Thanks to HD the PID Is used to run my charcoal smoker.
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Re: Recent Locked Thread

Post by Dancing4dan »

:D :D :) :)
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Re: Recent Locked Thread

Post by IMALOSERSCUMBAG »

Speaking of PID controllers....... Nope, not going there. I'm safer talking about Religion.😜
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Re: Recent Locked Thread

Post by cranky »

LWTCS wrote: Wed Mar 16, 2022 5:50 am I dont remember which one exactly yummy. It was one of those many debates about the use of PID for batch distillation.
A relatively new member had basically put far too much stock into what George was preaching.

As I recall the member wasn't taking the info provided here very well and things got heated. So the thread got locked because it turned into more of an argument more than a debate.
I'm pretty sure it was this train wreck of a thread by Cayers
viewtopic.php?f=85&t=77252
The last page is where the quotes came from
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Re: Recent Locked Thread

Post by LWTCS »

cranky wrote: Wed Mar 16, 2022 2:44 pm
LWTCS wrote: Wed Mar 16, 2022 5:50 am I dont remember which one exactly yummy. It was one of those many debates about the use of PID for batch distillation.
A relatively new member had basically put far too much stock into what George was preaching.

As I recall the member wasn't taking the info provided here very well and things got heated. So the thread got locked because it turned into more of an argument more than a debate.
I'm pretty sure it was this train wreck of a thread by Cayers
viewtopic.php?f=85&t=77252
The last page is where the quotes came from
Ah thanks.
Yeah he (cayers) was another engineer that couldn't make the cross over.
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Re: Recent Locked Thread

Post by cranky »

LWTCS wrote: Wed Mar 16, 2022 2:57 pm Ah thanks.
Yeah he (cayers) was another engineer that couldn't make the cross over.
So many of George Duncan's disciples couldn't make that cross over.

I was so tempted to buy a PID and video running my 3.5" glass CM the way those guys were claiming how to run it and another showing it running with my SSR but I'm not willing to waste $50 just to prove the point. If my youtube channel was dedicaed to distilling I probably would have.
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Re: Recent Locked Thread

Post by Wyododge »

I read the original post, I’ve seen the YouTube stuff, been reading here for some time. Don’t know enough to comment on them. All I know is the 8 or 10 people who I showed this information were both surprised and pissed. Most had been sold the same bill o goods. I’m with acrylic, gonna see if the brains of the family can get this printed and passed out. Lots of bulletin boards at grocery stores, co-ops and such. Heck, might even sneak one onto the bulletin board at the sheriff’s office for fun. You just never know who’s gonna read it.
It seems that discussions about alcohol percentage out of your still are remarkably similar to the MPG of your truck.
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Re: Recent Locked Thread

Post by drmiller100 »

That was indeed a great post and I totally agree.

I think this is an incredibly important topic.

I came to understand it slightly differently and perhaps my explanation might help someone.

Imagine a pot reflux still. The boiler has 10 percent etoh and is boiling. The top of the column is producing 95 percent.

Anywhere on the column in the packing between these two limits is somewhere between 50 and 95 percent Etoh.

The temperature will be between 172 and 195 ish.

Find the temp and you can use the chart to find the etoh concentration.

The chart is magic and very powerful.

Again, I offer this respectfully.
Now I know how you claim azeo so easy, it's based on a meat thermometer. :lol:
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Re: Recent Locked Thread

Post by Dancing4dan »

drmiller100 wrote: Sun Mar 20, 2022 6:51 pm “Imagine a pot reflux still” …… “ish” …..”The chart is magic and very powerful.”
:shock: WHAT? :wtf:

:ebiggrin: :ebiggrin: :ebiggrin:

I have so much more to learn!
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Re: Recent Locked Thread

Post by drmiller100 »

Dancing4dan wrote: Sun Mar 20, 2022 7:45 pm
drmiller100 wrote: Sun Mar 20, 2022 6:51 pm “Imagine a pot reflux still” …… “ish” …..”The chart is magic and very powerful.”
:shock: WHAT? :wtf:

:ebiggrin: :ebiggrin: :ebiggrin:

I have so much more to learn!
Lol!!! Yeah, I was being lazy and you caught me!!!!!
Now I know how you claim azeo so easy, it's based on a meat thermometer. :lol:
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Re: Recent Locked Thread

Post by Saltbush Bill »

What is a pot reflux still, its either one or the other imo.
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Re: Recent Locked Thread

Post by football29 »

Saltbush Bill wrote: Sun Mar 20, 2022 8:26 pm What is a pot reflux still, its either one or the other imo.
I think he means Pot = Batch reflux still. compared to Continuous Stripping + Rectification Still.

I say this as someone reading his entire post history trying to learn his knowledge.
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Re: Recent Locked Thread

Post by drmiller100 »

Saltbush Bill wrote: Sun Mar 20, 2022 8:26 pm What is a pot reflux still, its either one or the other imo.
Sorry. You are right. My mind is wandering tonight.
Now I know how you claim azeo so easy, it's based on a meat thermometer. :lol:
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