Many thanks

Putting older posts here. Going to try to keep the novice forum pruned about 90 days work. The 'good' old stuff is going to be put into appropriate forums.

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Prana
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Posts: 4
Joined: Tue May 05, 2009 3:20 pm
Location: Auckland

Many thanks

Post by Prana »

:D Decided to give a 2" VM column a go having looked through the information here and on the parent site. Realize I have a long, long way to go, but just wanted to say thanks for all the ideas and help I have received so far. Special mention ( in no particular order!) to HookLine, Rad, minime and punkin plus everyone else that has contributed to this forum.
I built a 160cm column, 130 cm SS scrubbers, 25mm take off reducing down to 15mm. Using a 50l beer keg with a 2500W element. At present I have about 95% coming off on my first run. First 50ml cloudy and smelly, rest is coming off smelling pretty sweet at 1l/hr. Was going to use this as a practice run, have already done the vinegar/cheap wine runs so almost reluctant to throw this away (or use it for future cleaning runs).
Plan is to go for a neutral to start with, but I have a piece of 2" left so will more than likely build a setup for pot distilling.
Attached is a couple of photo's, hope they work OK, smallest I could get them on Picassa.
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1/4" coil, used salt as recommended and managed this as my first attempt, not the prettiest, but works a treat.
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Liebig is crimped 15mm interior, 20mm outer and about 700mm long. A bit of overkill but who knows where the future lies 8)
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No points for guessing who's parrot I copied, very exciting watching the alcoholmeter settling at 95%!! Don't let the drop into the jar be too great or the liquid splashes out!!
Anyway, hope anyone just starting out realizes that with the help on this site and the main site there are all the tools required to get started fairly quickly.
Hawke
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Joined: Tue Mar 25, 2008 1:39 am

Re: Many thanks

Post by Hawke »

Prana wrote::D Don't let the drop into the jar be too great or the liquid splashes out!!
Anyway, hope anyone just starting out realizes that with the help on this site and the main site there are all the tools required to get started fairly quickly.
If you ran some cheap wine through it, this run could be a keeper.
For Mason jars and similar, I use a canning funnel over the jar. For small neck bottles and jugs, I have a funnel made from a 2x1/2 reducer. Keeps the splash from getting away.
Looks like you are well on your way.
It is the very things that we think we know, that keep us from learning what we should know.
Valved Reflux, 3"x54" Bok 'mini', 2 liebig based pots and the 'Blockhead' 60K btu propane heat
HookLine
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Joined: Sun May 13, 2007 8:38 am
Location: OzLand

Re: Many thanks

Post by HookLine »

Welcome and congrats.
Plan is to go for a neutral to start with, but I have a piece of 2" left so will more than likely build a setup for pot distilling.
Do it. Even if you never make flavoured spirits (and you almost certainly will end up making some), a simple pot head is very useful just for doing low wine (stripping) runs.
Be safe.
Be discreet.
And have fun.
rad14701
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Joined: Wed Dec 19, 2007 4:46 pm
Location: New York, USA

Re: Many thanks

Post by rad14701 »

Congratulations on the build, Prana...

You may be a bit limited on the take off rate due to the small branch size... The column:branch ratio is also loosely considered the minimum reflux ratio... By your description it sounds like a 2" column with a 1" branch which equates to a 4:1 theoretical minimum reflux based on area calculations... Having the 1" immediately reduce to 1/2" might marginally compound the issue... So, while you should be able to attain decent purity, your take off rate may be less than optimal but will get the job done...

Good luck...
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