Sugar wash ferments not performing well.. Help! :)

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Bobbydog
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Sugar wash ferments not performing well.. Help! :)

Post by Bobbydog »

Hello everyone, I hope you are all well. Happy new year too by the way :)

I have a couple sugar washes fermenting at the moment, and I'm not sure that they are performing up to thier maximum potential. It is only my second ferment ever, so I have very limited experience to work with. I would very much appreciate someone looking over these figures and letting me know if there is anything more that can be done to reduce the fermenting time without sacrificing the quality of the end product. Here are the facts:

70 litre rubbermaid totes with "semi" sealing lids (NOT air tight but snug fitting)
16 kg white sugar
1 small can (300ml ??) of tomato paste
3 tbls yeast nutrients
16 tbls realemon lemon juice
filtered well water with a starting PH of 7.0
225g regular bakers yeast / 80g Lalvin champagne yeast
water temp of 30 celcius maintained by a fish tank heater
starting S.G. of 1.070
very small submerged circulation pump, adding NO new air.

The water I'm using is from my well, and is known to have quite a bit of Iron in it. When the water comes in the house it goes through (2) sediment/iron filters, and then through (1) carbon filter. However I've never tested the output for iron content. I'm not sure that I can, or if its important at all. There is no off tastes to the water, so I've always just assumed that it was "clean". The PH of the water is 7.0 as tested with a swimming pool PH tester. I have one fermenting tank using the bakers yeast, and another tank using the Lalvin yeast.

I thought I had a pretty good wash, but its been 9 full days now and the S.G. is only at 1.050. Not exactly what I was looking for :( I have read this entire site. To the point now where I've read soo many different things that I'm not sure where I should be focusing my attention. I'm wondering what you old fellas would do first?

- Is my water the problem because of the high starting PH, or possibly the iron?
- Should I distill all my well water first?
- Is the "snug" fitting lid letting too much fresh air in?
- Is the circulation pump "grinding" up the yeast?
- Are the preservatives in the Realemon hampering the yeast?
- Am I adding enough tomato paste, yeast nutrients?
- Is 30 celcius too cold?
- Am I not taking the S.G. measurements properly?
- Am I missing an important nutrient all together? Epsom salts maybe?
- Maybe I should just be happy with what Im getting?


I am looking for a neutral spirit. My plan is to do strip runs and then double distill a full charge of the low wines. Finally running the product through carbon filters if need be.

Any input on any of these questions would be a great help. I find my confidence in my fermenting skills waivering and could sure use a boost :) Thanks in advance..

Bob
Dnderhead
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Re: Sugar wash ferments not performing well.. Help! :)

Post by Dnderhead »

as it is filterd it mite lack in minreals,, add as tea spoon of epsom salt, if it dont help it is not going to hurt.
rad14701
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Re: Sugar wash ferments not performing well.. Help! :)

Post by rad14701 »

It is only my second ferment ever, so I have very limited experience to work with.
If you've read the entire site then you should be aware that a novice shouldn't be trying to learn by mixing ingredients at random instead of using a Tried and True recipe... There's a reason why we suggest that novices start with them, the main reason being that they are predictable and problems are easily identified and resolved... All we know about your recipe is that you tossed in a little of this and a little of that, without any reasoning associated with each ingredient or quantity...

You've mentioned the size of the fermenter but not how much water was added or the total volume... My first guess would be not enough nutrients for the yeast to process 16kg of sugar... Second guess is that the wash is too cold... Beyond that, can't say... Epsom salt or 20-20-20 might help at ~1/4 teaspoon per gallon...

How warm was the water when the sugar was added...??? Did you invert the sugar...???

Good luck...

EDIT: Damned metrics and my typo created conversion error... 30C/86F is at about the upper end of temperature range, but not catastrophic...
Last edited by rad14701 on Wed Jan 13, 2010 2:40 pm, edited 2 times in total.
Barney Fife
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Re: Sugar wash ferments not performing well.. Help! :)

Post by Barney Fife »

Why the circulation pump? I've never heard of anyone stirring a wash while it ferments!

Other than that, yes, the realemon isn't too good, and you used quite a bit. Just buy a lemon and squeeze it next time you need acid. And yes, you're quite short on nutrients with just that one small can of paste. You're making a triple sized wash, so triple the nutrients, also.

I'd add -something- to feed the yeast, like a few more cans of paste, or a energy drink or two, or a pound or two of cracked corn, anything. Then I'd make a new yeast starter using about a quart(liter) of the wash that I would shake like hell the get plenty of air into, along with a new handful of yeast. Once this starter got going, I'd pour it into the fermenter from a few feet above, so it adds more air to the wash as it enters. She'd go like hell after that....

30C(86F) is actually a bit hot. 20C is fine.
Bobbydog
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Re: Sugar wash ferments not performing well.. Help! :)

Post by Bobbydog »

- The fermenting tanks hold 70 litres total of wash. (The tanks have a capacity of 100 litres)
- I dissolved the sugar in 40 litres boiling water, stirring the hell out of it.
- I added the tomato and nutrients, then topped the fermenter up to 70 litres with water to achieve a water temp of 36C.
- I sprinkled the yeast on the surface with a wash temperature of 36C. (the yeast packages recommended 30-40C.)
- I aerated the wash just prior to pitching the yeast.
- I used enough Realemon to bring the washes PH down to 6.0, from what Ive read 4.8 is the ideal PH, however I didnt feel comfortable adding any more lemon juice.
- I used 1 tbls of packaged nutrients per 22 litres wash as per the instructions on the bag. The package contains DAP, yeast hulls, vitamin B complex, magnesium sulphate.

My tanks are outside of the house. (I'm still working on the wife) They are insulated very well but at night it gets down to -10 celcius. My worry is that I will get a "cold spot" on the side opposite the fish tank heater, so this is the main reason I use the recirc pump. It is also recommended in the book written by Dr.Stone called "Making Gin and Vodka".

The first wash I ever made was the standard 5 kilos sugar and 70 grams of bakers yeast for 20 litres volume of water. It went without a hitch however it was in a totally different house, in a different tank inside the house, in the summer. I was hoping that these "extras" such as nutrients and tomato paste would ensure a full ferment. From what I have read, many people have had troubles with simple sugar washes without adding nutrients. I was hoping to prevent that..

Next wash I will use river water from across the street, and I'll use real lemons or packaged citric acid if needed to get the PH down to 5.0 if possible. After these batches are done, I'll test the theory of the "cold spots" and see if I cant eliminate the circ pump altogether. I'll also pick up some Epsom salts if nobody here thinks it could "hurt".

Thanks for the input, I'll get er eventually.. :)

Bob
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Re: Sugar wash ferments not performing well.. Help! :)

Post by Dnderhead »

Id say stay away from "realemon" the heater will be fine with out the pump.
the nutrients I have say 2.6 g per. l of 14%
Barney Fife
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Re: Sugar wash ferments not performing well.. Help! :)

Post by Barney Fife »

From what I have read, many people have had troubles with simple sugar washes without adding nutrients. I was hoping to prevent that..

Yeast can't live on sugar; they "eat" sugar to get the oxygen they need so's not to drown. The need nutrients to eat for energy. A plain sugar wash will only ferment for as long the yeast you added lived, which isn't too long, and they won't multiply when they're starving, so what you put in, is all ya got. Add nutrients and oxygen, the yeast multiply like rabbits on Viagra until they use up all the oxygen, then the now huge colony of yeasties think, "oh shit, what do I do now!!", and they realize that there's an oxygen molecule in the sugar they have all around them. Smart bastards! So they munch on that for oxygen, but they still need to eat the nutrients for energy. Just like you and I, no matter how much air we have, we're screwed if we don't eat something at some point.

Get it? ;)
Barney Fife
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Re: Sugar wash ferments not performing well.. Help! :)

Post by Barney Fife »

Hmm.... somehow, we can no longer edit our posts?

At any rate, it's not a oxygen "atom" but a molecule or whatever that the yeast get from the sugars.

Wassup with editing?
Bobbydog
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Re: Sugar wash ferments not performing well.. Help! :)

Post by Bobbydog »

I gave the wash 12 days, the S.G. was still at 1.050 so I'm fairly certain that I had a major problem. :) I ran both washes through the still and only managed to get a couple litres. Such is life. I've started a new wash and I feel pretty good about this one. 10 minutes after I added the yeast I could actually see the wash "boiling". Almost like there was a small circ pump under the surface. I never had that reaction on any of the first three I've made, I'm hoping that is a good sign.. Anyway, heres the new ingredient list. Thanks for everyones input.

15 kg white sugar
(3) 200ml cans tomato paste
4 Tbsp packaged yeast nutrients
4 fresh lemons juice
1 tsp epsom salts
1 tsp packaged acid blend to bring the PH down to 5.0
225 grams Flieshmans bakers yeast
Add river water to bring total wash to 70 litres
Starting S.G. of 1.070
Wash temperature maintained at 30 Celcius

I'll be sure to post the results in a few days. I'm trying not to get too confident, but I feel good about this one. Thanks again.. :)


Bob
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Re: Sugar wash ferments not performing well.. Help! :)

Post by olddog »

That recipe sounds about right. :D
OLD DOG LEARNING NEW TRICKS ......
HookLine
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Re: Sugar wash ferments not performing well.. Help! :)

Post by HookLine »

Barney Fife wrote:Hmm.... somehow, we can no longer edit our posts?

Wassup with editing?
You only got a short time frame after your post to edit it. After that only mods/admins can edit.

Edited it for you.
Be safe.
Be discreet.
And have fun.
Bobbydog
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Re: Sugar wash ferments not performing well.. Help! :)

Post by Bobbydog »

So far soo good. I just checked the wash and its got a S.G. of 1.040! Thats just after 2 days :) I'm pretty happy with that progress to say the least. The wash had foamed up high enough to reach the lid which has never happened to me before. I'm not using the recirp pump for this wash, but I just checked the water temps and they are even throughout the tank. That is great news. One thing I am noticing though.. The plastic rubbermaid totes are starting to lose shape and the lid is no longer "snapping" on as well. I can see that I will have to replace them with something more sturdy in the near future. Maybe some good heavy garbage cans with duct tape wrapped around the top edge of the can to hold the round shapes diameter? Now that I think of it , some big beer coolers would be even better. They have hinged lids already, and they are insulated which is a bonus to us fermenting outside in the cold. Anyway, I'll give another update in a few days. Thanks for the input.

Bob
SaltUbar
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Re: Sugar wash ferments not performing well.. Help! :)

Post by SaltUbar »

Hi there,

You should really go and look at the tried and true receipe. I can recomend the wino's ye old sugar wash it works great.

Regards Ubar
If you always do what you have always done, you will always get what you have always got
Bobbydog
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Re: Sugar wash ferments not performing well.. Help! :)

Post by Bobbydog »

This is Wineos sugar wash.. At least I thought it was. The only thing he used that I didnt was the gypsom, I'll give that a go next batch. My washes have slowed considerably since the first two days, and I noticed that everything that was floating on the surface over the last 5 days has sank to the bottom leaving a pretty much "clear" liquid. I'm guessing that my yeast is dead. The wash is still sweet, and the S.G. is at 1.020. If the S.G. doesnt move again tomorrow I'll run that batch through and start a new one. I was going to throw some more yeast in there but I'd rather get this one over with and start a fresh one indoors. I tested the water temp and it was only at 26 celcius. I have the heaters set at 30 but its been bitterly cold here the last few days, so indoors is the only way to go. The rubbermaid totes that I'm using are too messy so I'm shopping around for something better to use. I have a couple of plastic 200 litre (50 gal) "oil" drums that I could use, but I'm not sure I want to tackle a 180 litre wash just yet :) I still need to figure out why my yeast keeps dying lol..

If anyone has any other ideas I'd love to hear them, thanks in advance. :)

Bob
Bobbydog
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Re: Sugar wash ferments not performing well.. Help! :)

Post by Bobbydog »

I think that I've figured out my problem(s).

The first mistake I made was boiling 40 litres of water for a 70 litre wash. I had no idea that boiling water removes ALL of the oxygen from the water. Therefore I have been using "dead" water for my washes. I read somewhere that boiling water is better for dissolving sugar so I went a little overboard there. My new plan is to heat up, not boil, only 20 litres of water for dissolving the sugar with.

The second mistake I made was not removing all of the iron from my water. I read all sorts of literature last night on how high iron levels can negatively affect yeast, and I KNOW that I have really high iron levels in my area. There are only two ways to remove soluble iron from water from what I read, one is to inject air into your water system, oxydizing (rusting) the soluble (ferrous) iron into non-soluble (ferric) iron. Then running the water through a filter. The other way is to buy an expensive filter that has a special coating which oxidizes the soluble iron on contact.

My new plan is to install a bubbler hose in the bottom of a 1000 litre tank I have, then fill it with river water and bubble the hell out of it for a day. That should oxygenate the water as well as remove any soluble iron from the water. Then I'll just pump that through a regular sediment filter. Additionally, I'll pick up a fish tank bubbler stone and throw that into my fermenting tank. I'll pump air through it for an hour or so after adding the yeast to the wash, and then I'll do the same for an hour the day after as well. After that I'll slap the lid on and hope for the best :)

I'm hoping that these two improvements will allow my yeast to multiply to a point where I can get a full ferment from a wash before they all die.

What do you guys think? Am I making any sense here? lol.. I'll let you know how my next wash performs.

Bob
rad14701
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Re: Sugar wash ferments not performing well.. Help! :)

Post by rad14701 »

Bobbydog, boiling the water to invert sugar does remove the oxygen, which is why we aerate our washes before and/or after pitching our yeast... It may or may not also help with the iron issue... Probably not when you consider that we only boil enough water to invert the sugar, not all of the water...

Did some quick Googling and found that experimentation has been done to remove iron and arsenic from water using rare earth magnets... Might be worth investigating...
SaltUbar
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Re: Sugar wash ferments not performing well.. Help! :)

Post by SaltUbar »

Hi Bobbydog,

I have been experimenting with Wino’s sugar wash using the recipe exactly but changing one thing at a time. I have found the following;

1. Increasing the DAP x 2 slows down the fermentation;
2. Boiling the water prier to pitching yeast results in significant slowing of fermentation
3. Adding spent yeast prior to pitching doesn’t make any difference
4. Adding a vitamin B complex pill speeds up ferment greatly
5. Keeping the temp at or around 30 degrees C is the best
6. Aerating the wash by stirring vigorously prior to pitching really helps yeast multiplication
(frothed up through the air trap and out of the 55lt barrel I am using)

I am currently trying to keep the Ph above 5 by adding Calcium Carbonate as the fermentation works. I have added 7 teaspoons on my current wash but it didn’t seam to make much difference. Although I was not successful in making the Ph go much higher than 4 I am going to try again with another wash to see if i can keep the ferment going more vigerously at the tail end of the fermentation. The current wash has gone from an SG of 1.058 to 1.012 in 4.9 days

Interested to know what you are trying.

Regards Ubar
If you always do what you have always done, you will always get what you have always got
Dnderhead
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Re: Sugar wash ferments not performing well.. Help! :)

Post by Dnderhead »

if you are going to use spent yeast as a nutrient boil the them first, I like to add the yeast to boiling water(a deep pot) as you need the contents of their little bellies.
your wash is going to slow down as most of the sugar is gone.
Bobbydog
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Re: Sugar wash ferments not performing well.. Help! :)

Post by Bobbydog »

Hello everyone.

I thought that I should give a bit of an update to this thread, for those of you that have read through it.

I have a good handle on sugar washes now, thanks to all the help from this forum and the mother site. I can get a consistant 7 to 8 litres of 95% from my 70 litre washes now.
Many of my fears in the beginning were for nothing, and I underestimated a few very important things. Heres what I needed to know to semi/fully understand whats going on...

- Yeast is an organisim that has needs just like us. It needs oxygen to breath, food to eat, and a nice warm place to call home. In nature wild yeast grows on tomatoes and grapes. NOT underwater. It is a very resourceful creature, it has the ability to steal the oxygen from sugar to breath. We are exploiting this unique ability by "drowning" these poor little buggers in our wash. However, they dont drown the second you put them in the wash. They can live quite happily and even mulitply by the millions when there is easy "free" oxygen floating around in your wash. As soon as the "free" oxygen in the wash is used up, the yeast starts to drown and stops all multiplying. (This takes from a couple hours to a couple days, but for most people this will be around half a day) It then switches to the much harder job of "breathing" the oxygen out of the sugar, which leaves us with an equal amount of both CO2 and Ethanol. The CO2 floats off into the atmosphere and the ethanol starts to concentrate in the wash. Heres the kicker, this ethanol "piss" is toxic to the yeast. No yeast on earth can live in a concentration past 20% ethanol by volume. During all of this process, the yeast MUST STILL BE FED nitrogen. Or else breathing oxygen isnt going to be their problem anymore, cause they will be dead from starvation. As long as you have a "cap" of foam on the surface of your wash, your yeast colony is still alive and trying to breath the sugar and eat the nitrogen. When the foam cap starts to break up and sink, you are either out of sugar to breath, out of nitrogen to eat, or have a lethal amount of ethanol in the wash. The real trick is trying to time all of these processes so that we get the most amount of good clean ethanol.
- There are many foods that yeast can eat, but the thing that is essential in all yeast foods is the nitrogen content. The simplest of these is DAP which is just a chemical nitrogen source. Really no different than fertilizing your lawn.
- Anything added other than oxygen, sugar, and a nitrogen source are an attempt to make the yeasts lives a little easier. (e.g. Vitamin B) They are not required to "get the job done". The easier we can make their lives, the less nasty flavours we'll get, and the quicker the yeast can finish "breathing" all the sugar up.

So heres the process I use for a 70 litre wash.

Boil for 1 hour, 15kg sugar with 8 litres of water ( yes it really dissolves in that little amount of water) and 3 teaspoons of packaged acid blend (tartaric/citric). A real slow boil without the lid is how I do it. Cost: $16 Cdn
Add this to your tub, then add (2) 300ml cans of tomato paste for a food source. Cost: $3 Cdn
Add 6 Tablespoons packaged yeast nutirents (Dap, yeast hulls, etc) for a food source. Cost: $1.50 Cdn
Add 1 teaspoon epsom salts
Add 1 teaspoon soluble Miracle grow 20-20-20 for a food source and trace minerals. Look for a fertilizer that lists "Di-ammonium Phosphate" as the nitrogen source. Its getting hard to find here in Canada. All I see now is "Phosphate free" on the label. Its not critical to get the DAP, its just the best for yeast. If its not DAP its Urea which is fine in small amounts like were using. Keep in mind that you are trying to grow and organism, just like the carrots in your garden.
Add water until you get 70 litres total wash.
Stir everything like a madman for about 3 or 4 minutes with a large wisk. Doing your best to incorporate air into the wash.
Add a large size fish tank heater and set it to 30 celcius. Leave the wash overnight to equalize at 30 deg celcius.
The next morning, warm to 38 Celcius (use a thermometer!) 2 litres of clean water in a 5 litre bowl. (You can pitch the yeast directly into your wash at this point, but the survivabliity rate of the yeast is much higher if they are rehydrated in clean water)
Gently wisk the water as you slowly add 1 bag of bakers instant yeast. (450ml) Cost: $8.50 Cdn
Let the yeast sit for a half hour. It will grow alot so keep an eye on it!
Wisk the wash for a couple minutes and then pour the yeast into the wash.
Add a floating thermometer and put a loosely covered lid on the whole thing. Check the temp once a day to make sure your heater hasnt packed it in.

Within minutes you will start to see bubbles and the whole thing will go crazy forming a "cap" on the surface. This is a good thing.
What happens now is your yeast will have everything it needs to multiply. The "free" oxygen you stirred in, the food sources, and heat. Its not too concerned about the sugar at this point, as long as its not too thick a syrup (1.08 with a hydrometer)
The yeast will spend the next few hours multiplying like rabbits on ecstacy, to a point where they use up all the "free" oxygen.
This is where the yeast stop multiplying, so whatever army of yeast you have in there at this point is all you get. Keep in mind that you must FEED AN ARMY.
The yeast start to break down the sugar to breath, creating CO2 and ethanol. All the while eating up all the nutients you added in the beginning.

So I keep these things in mind now..

If the yeast runs out of food to eat or sugar to breath, they will die.
If the yeast get too cold or hot, they will die.
If the yeast create too much ethanol, they will die.

I dont worry about things like a tight fitting lid, aerating, vitamins, daily stirring, types of yeast, or anything else really. All of these things will give you small improvements, that you can play around with once you get to know your system.
I just watch the "cap" of the wash, it will tell you if everything is working the way its supposed too. One time I had the cap start to sink after 5 days at a hydrometer reading of 1.02. So I added 2 tablespoons of yeast nutrients and gave it a stir. Within an hour I had a new cap, and the wash finished out to .99 in two more days. I might be wrong, but I'm going to assume that the biggest challenge is keeping the yeast well fed until the point that they create so much ethanol they poison themselves. Which by the way is also the point at which you want them to run out of sugar to breath.

Anyway, I'm getting tired of typing and I have a batch running through atm, so I'll leave it at that and if anyone has any questions please feel free to ask. Thanks again to everyone here for all their help :)

Bob
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